Double-component waterborne polyurethane glass transparent insulating coating
A technology for water-based polyurethane and heat-insulating coatings, applied in the field of coatings, can solve the problems of unsatisfactory performance of water-based glass heat-insulating coatings, and achieve the effect of improving low hardness and high infrared reflectivity
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specific Embodiment approach
[0039] The specific implementation method: two-component water-based polyurethane glass transparent heat-insulating coating, its formula ratio is (percentage by weight):
[0040] Acrylic Dispersion:
[0041]
[0042] Put 50g of acetone into a four-neck flask equipped with a stirring blade and a condenser tube, raise the temperature to 80°C with a heating mantle, then add 5g of methyl methacrylate, 15g of hydroxyethyl methacrylate, 10g of butyl acrylate, and methacrylic acid Put the mixture of 5g and 1.5g di-tert-butyl peroxide into the constant pressure funnel, drop it into the four-necked bottle in 2-3h, add 0.5g di-tert-butyl peroxide after the dropwise addition and react for 2h, then lower the temperature to 60 ℃, neutralized with TEA to pH 7-8, and then added 63g of distilled water. The solvent was distilled off under reduced pressure to obtain a self-synthesized acrylic acid dispersion.
[0043] Thermal insulation coating:
[0044]
[0045] Take 39g of distilled ...
Embodiment 2
[0047] The specific implementation method: two-component water-based polyurethane glass transparent heat-insulating coating, its formula ratio is (percentage by weight):
[0048] Acrylic Dispersion:
[0049]
[0050] Put 50g of acetone into a four-necked flask equipped with a stirring blade and a condenser tube, raise the temperature to 80°C with a heating mantle, then add 10g of methyl methacrylate, 20g of hydroxyethyl methacrylate, 10g of butyl acrylate, and methacrylic acid Put the mixture of 10g and 4.5g of di-tert-butyl peroxide into a constant pressure funnel, drop it into a four-necked bottle in 2-3 hours, add 0.5g of di-tert-butyl peroxide after the addition and react for 2 hours, then cool down to 60 ℃, neutralized with TEA to pH 7-8, and then added 45 g of distilled water. The solvent was distilled off under reduced pressure to obtain a self-synthesized acrylic acid dispersion.
[0051] Thermal insulation coating:
[0052]
[0053] Take 7g of distilled water, ...
Embodiment 3
[0055] The specific implementation method: two-component water-based polyurethane glass transparent heat-insulating coating, its formula ratio is (percentage by weight):
[0056] Acrylic Dispersion:
[0057]
[0058] Put 50g of acetone into a four-necked flask equipped with a stirring blade and a condenser tube, raise the temperature to 80°C with a heating mantle, then add 10g of methyl methacrylate, 15g of hydroxyethyl methacrylate, 15g of butyl acrylate, methacrylic acid Put the mixture of 7g and 2.5g di-tert-butyl peroxide into the constant pressure funnel, drop it into the four-necked bottle in 2-3h, add 0.5g di-tert-butyl peroxide after the dropwise addition and react for 2h, then lower the temperature to 60 ℃, neutralized with TEA to pH 7-8, and then added 50 g of distilled water. The solvent was distilled off under reduced pressure to obtain a self-synthesized acrylic acid dispersion.
[0059] Thermal insulation coating:
[0060]
[0061] Take 20.7g of distille...
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Abstract
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