Detection method for pharmaceutic preparation containing sanguis draconis extract
A technology of pharmaceutical preparations and detection methods, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of few detection items, thin layer identification and insufficient accuracy of spectrophotometry, etc.
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Embodiment 1
[0285] Embodiment 1: the content determination method of total phenol:
[0286] a. Preparation of the reference substance solution: take an appropriate amount of 7,4′-dihydroxyflavone, accurately weigh it, put it in a brown measuring bottle, add absolute ethanol to make a solution containing 28 μg per 1 ml, and obtain it;
[0287] b. Preparation of standard curve: Accurately measure reference substance solution 0, 1.0, 2.0, 3.0, 4.0, 5.0ml, put them in 25ml measuring bottles respectively, add absolute ethanol to 5ml, add 0.3% dodecylsulfonic acid Sodium solution 2ml, 0.6% potassium ferricyanide solution 1ml, 0.9% ferric chloride solution 1ml, shake well, put it in a dark place for 5min, add 0.1M hydrochloric acid to the mark, shake well, put it away from light Place it for 35 minutes, and take the first copy as a blank; according to the UV-visible spectrophotometry method of Appendix VB of the Chinese Pharmacopoeia in 2005, measure the absorbance at 760nm, take the absorbance ...
Embodiment 2
[0290] Embodiment 2: the content assay method of total phenol:
[0291] a. Preparation of the reference substance solution: take an appropriate amount of 7,4′-dihydroxyflavone, accurately weigh it, put it in a brown measuring bottle, add absolute ethanol to make a solution containing 32 μg per 1 ml, and obtain it;
[0292] b. Preparation of standard curve: Accurately measure reference substance solution 0, 1.0, 2.0, 3.0, 4.0, 5.0ml, put them in 25ml measuring bottles respectively, add absolute ethanol to 5ml, add 0.3% dodecylsulfonic acid Sodium solution 2ml, 0.6% potassium ferricyanide solution 1ml, 0.9% ferric chloride solution 1ml, shake well, put it in a dark place for 5min, add 0.1M hydrochloric acid to the mark, shake well, put it away from light place at 780nm according to the ultraviolet-visible spectrophotometry method of appendix VB of the Chinese Pharmacopoeia in 2005, measure the absorbance at 780nm, take the absorbance as the ordinate, and the concentration as the...
Embodiment 3
[0295] Embodiment 3: the assay method of total phenol content:
[0296] a. Preparation of the reference substance solution: take an appropriate amount of 7,4′-dihydroxyflavone, accurately weigh it, put it in a brown measuring bottle, add absolute ethanol to make a solution containing 36 μg per 1 ml, and obtain it;
[0297] b. Preparation of standard curve: Accurately measure reference substance solution 0, 1.0, 2.0, 3.0, 4.0, 5.0ml, put them in 25ml measuring bottles respectively, add absolute ethanol to 5ml, add 0.3% dodecylsulfonic acid Sodium solution 2ml, 0.6% potassium ferricyanide solution 1ml, 0.9% ferric chloride solution 1ml, shake well, put it in a dark place for 5min, add 0.1M hydrochloric acid to the mark, shake well, put it away from light Place it for 35 minutes, and take the first copy as a blank; according to the ultraviolet-visible spectrophotometry method of appendix VB of the Chinese Pharmacopoeia in 2005, measure the absorbance at 800nm, take the absorbance...
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