Polyester waterproof ventilated membrane, three-layer compound material, preparation method and application thereof
A technology of waterproof, breathable and composite materials, which is applied in the direction of roof insulation materials, building insulation materials, chemical instruments and methods, etc., can solve the problems that have not been reported in public, and achieve the effect of excellent waterproof, breathable and moisture-permeable functions, and good strength performance
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Embodiment 1
[0031] Use PET (PG620, Yizheng Chemical Fiber Co., Ltd.) 60Kg, PTT (FG30, U.S. Shell Company) 10Kg, PBT (B4406, Germany BASF) 10Kg with a polyester chip fluidized bed crystallization dryer (FBCD type, Zhangjiagang City Tenglong) Machinery Manufacturing Co., Ltd.) crystallization drying, the pre-crystallization temperature is 140°C, the time is 0.5 hours, the drying temperature is 160°C, the drying time is 4 hours, and the residual water content is <35ppm.
[0032]Dry and dehydrate 20Kg of PETG (0603, American Eastman Company) with a double-cone rotary vacuum dryer (GZS type, Hangzhou Qianjiang Drying Equipment Co., Ltd.), the ultimate vacuum is ≤ 3Pa, the drying temperature is 90-100 ° C, and the time is 4 hours. Residual water content ≤ 30ppm;
[0033] Dry and dehydrate 140Kg of heavy calcium carbonate (particle size 3-5 μm, HT-1500, Zhejiang Changxing Dadi New Material Co., Ltd.) with a double-cone rotary vacuum dryer (GZS type, Hangzhou Qianjiang Drying Equipment Co., Ltd.)...
Embodiment 2
[0038] PCTG (0618, U.S. Eastman Company) 20Kg substitutes the PETG in the embodiment 1 after the method drying dehydration of embodiment 1, all the other raw materials and used weight parts, dry dehydration, mixing, granulation, casting, stretching preparation The process and conditions of the microporous membrane and the preparation of the three-layer composite material are the same as in Example 1.
Embodiment 3
[0040] The montmorillonite (3~5 μm of particle size, JT-518, Jintai Bentonite Co., Ltd., Anji County, Zhejiang Province) 150Kg after the method drying dehydration of Example 1 replaces the heavy calcium carbonate in Example 1, with coupling agent vinyl Trimethoxysilane (A-171, Nanjing Yudeheng Fine Chemical Co., Ltd.) 2Kg replaces the coupling agent aluminate and titanate in Example 1, the rest of the raw materials and parts by weight, drying and dehydration, mixing, granulation , casting, stretching to prepare microporous film and prepare the technological process and conditions of three-layer composite material with embodiment 1.
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