Preparation of aluminum phosphate or polyphosphate particles
A technology of aluminum polyphosphate and aluminum phosphate, applied in phosphorus compounds, inorganic chemistry, fibrous fillers, etc., can solve the problems of high cost and so on
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Embodiment 1
[0072] Preparation of aluminum phosphate powder
[0073] 791g phosphoric acid (81.9% by weight of H 3 PO 4 or 59.3 wt% P 2 o 5 ) and 189g of hydrated aluminum hydroxide (85.3% by weight of Al(OH) 3 or 58.1 wt% Al 2 o 3 ) was reacted in 210 g of water at 80° C. for 1 hour (P / Al final molar ratio=2.99) to obtain an acidic aluminum phosphate solution. In the second step, 1155 g of commercially purified sodium aluminate solution (9.7 wt% Al and 11.2 wt% Na, or 18.3 wt% Al 2 o 3 and 15.7 wt% Na 2 O, final Na / Al=1.36) and acidic aluminum phosphate solution were simultaneously added to a stirred vessel filled with 1500 g of water at room temperature.
[0074] The final reaction pH was 7.1 and the temperature during the reaction was maintained at 45°C. The resulting dispersion was centrifuged (30 minutes, 2500rpm—relative centrifugal force: 1822g) to remove the reaction mother liquor to form a filter cake, which was washed once with water (1000g of washing water) to obtain a...
Embodiment 2
[0076] Preparation of Aluminum Phosphate Slurry
[0077] 10.0 g of water was added to a 250 mL beaker. During mixing at 800 RPM (Cowles), add about 1.34 g (1% of non-volatile content) of sodium polyphosphate. After 5 minutes, 150.0 g of aluminum phosphate slurry (30% non-volatiles) was added slowly (25 g / min). After another 5 minutes, the agitation speed was increased to 1800 RPM and 109.0 g of aluminum phosphate powder (80% non-volatiles) were added slowly (10 g / min). After powder addition, the slurry was kept stirring at 1800 RPM for 20 minutes.
Embodiment 3
[0079] Preparation of Aluminum Phosphate Slurry
[0080] 72.0 g of water was added to a 250 mL beaker. During mixing at 800 RPM (Cowles), about 0.96 g (1% of non-volatile content) of sodium polyphosphate was added. After 5 minutes, the agitation speed was increased to 1800 RPM and 122.0 g of aluminum phosphate powder (80% non-volatiles) was added slowly (10 g / min). After powder addition, the slurry was held at 1800 RPM for 20 minutes.
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