Iron-based soft magnetic powder for dust core, production method thereof, and dust core
A powder magnetic core and soft magnetic technology, which is applied in the manufacture of inductors/transformers/magnets, magnetic cores/yokes, transformers/inductor cores, etc., can solve the problem of increased eddy current loss and electrical insulation of powder magnetic cores Insufficient problems, such as low iron loss, improved heat resistance, and high magnetic flux density
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Embodiment 1
[0047] Pure iron powder (manufactured by Kobe Steel, Atmel 300NH, average particle diameter 80 to 100 μm) was used as the soft magnetic powder. Water: 1000 parts, Na 2 HPO 4 : 88.5 parts, H 3 PO 4 : 181 copies, H 2 SO 4 : 61 copies, Co 3 (PO 4 ) 2 : 30 parts, Cs 2 SO 4 : 44 parts were mixed, and 10 parts of the 10-fold diluted treatment solution was added to 200 parts of the above-mentioned pure iron powder passing through a sieve with a mesh size of 300 μm, mixed with a V-type mixer for 30 minutes, and then dried at 200°C in the atmosphere After 30 minutes, pass through a sieve with a mesh size of 300 μm.
[0048] Next, a silicone resin "KR220L" (manufactured by Shin-Etsu Chemical Co., Ltd.) with 100 mol% of methyl groups and 100 mol% of T units was dissolved in toluene to prepare a resin solution with a solid content concentration of 4.8%. This resin solution was added and mixed so that the resin solid content was 0.15% with respect to the iron powder, heated in a...
Embodiment 2~4
[0052] Embodiment 2~4, comparative example 1
[0053] As shown in Table 1, except that the composition of the treatment liquid was changed, the compressed powder compact was produced in the same manner as in Example 1, and the element content, compact density, flexural strength, and specific resistance were measured, and are shown in Table 2 and Table 3. .
[0054] 【Table 1】
[0055]
No.
phosphorylated coating
Add elements in
Na 2 HPO 4
NaH 2 PO 4
h 3 PO 4
co 3 (PO 4 ) 2
h 2 SO 4
Cs 2 SO 4
Al(H 2 PO 4 ) 3
Example 1
P, Co, Na,
S, Cs
88.5
—
181
30
61
44
—
Example 2
P, Co, Na,
S, Cs —
150
181
30
61
44
—
Example 3
P, Co, Na,
S, Al 88.5
—
181
30
61
—
78
Example 4 ...
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