Onion oil extraction method from onion leave using supercritical carbon dioxide method
A carbon dioxide and supercritical technology, which is applied in the direction of digestive system, pharmaceutical formulations, medical preparations containing active ingredients, etc., can solve the problems of low extraction efficiency and inability to solve organic solvent residues, etc., to achieve thorough extraction, good development prospects, selective effect
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[0027] (1) Raw materials: yellow onion leaves;
[0028] (2) drying: the onion blades are naturally dried;
[0029] (3) pulverizing: the dry onion leaves are pulverized and sieved to get the onion leaf powder with particle size <40 mesh;
[0030] (4) Supercritical CO 2 Extraction: Put 100kg of the dried onion leaves into HA121-50-01 supercritical extraction device (produced by Jiangsu Nantong Huaan Supercritical Extraction Co., Ltd.), adjust the extraction temperature, extraction pressure and extraction time to make it reach the optimum extraction parameter of 37.35°C , the extraction pressure is 27.5MPa, the extraction time is 57.9min, and the onion oil crude extract is directly collected in a brown jar at the outlet of the extraction kettle;
[0031] (5) Post-treatment: evaporate ethanol, extract the crude extract twice with dichloromethane at a volume ratio of 1:1 at 25°C, add activated carbon to remove pigments, and recover dichloromethane at 42°C;
[0032] (6) with anhy...
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