Method for preparing full biodegradable environment protection hot melt adhesive
A fully degradable, hot-melt adhesive technology, applied in the direction of adhesives, starch-derived adhesives, adhesive types, etc., to achieve the effects of low production cost, uniform phase, and simple and easy production methods
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Embodiment 1
[0021] Add 410 grams of cornstarch into the high blender, then add 20 grams of glycerin, 5 grams of PEG (400), 20 grams of sodium montmorillonite, 20 grams of ethyl cellulose, and 25 grams of calcium stearate. , 3000rpm high-speed stirring for 1 hour to discharge. Add 200 grams of PLA resin in the middle of the obtained modified starch, 150 grams of terpene resin, 100 grams of polyethylene wax, 40 grams of dioctyl phthalate, 10 grams of 2,6-di-tert-butyl p-cresol, Then stir and mix evenly at a low speed, add it to the preheated extruder hopper, set the temperature from the feed port to the head of the extruder at 120-180°C, and extrude at a screw speed of 80rpm, and the extruded product is granulated to obtain a hot melt adhesive. product.
Embodiment 2
[0023] Add 320 grams of cornstarch into the blender, then add 10 grams of glycerin, 15 grams of nickel-based montmorillonite, 10 grams of methyl cellulose, 20 grams of glyceryl monostearate, and 25 grams of calcium carbonate. , 1000rpm high-speed stirring for about 30 minutes to discharge. Add 300 grams of PCL, 240 grams of terpene resin, 50 grams of polyethylene wax, 10 grams of 4,4' thiobis (3-methyl-6-tert-butyl) phenol in the modified starch obtained, and then low speed Stir and mix evenly, add to the preheated extruder hopper, set the extrusion temperature at 100-150°C, and extrude at the screw speed of 200rpm, and the extruded product is granulated to obtain a hot melt adhesive product. The measured melting point is 160-165°C, and the initial shear strength is 25N / 5.0cm.
Embodiment 3
[0025] Add 400 grams of cornstarch into the high blender, then add 10 grams of urea, 20 grams of water, 5 grams of glyceryl monostearate, 15 grams of magnesium-based montmorillonite, 25 grams of cellulose acetate succinate, light calcium carbonate 25 grams, at a temperature of 50 ° C, 3000 rpm high-speed stirring for about 50 minutes to discharge. Add 200 grams of PBAT resin in the middle of the obtained modified starch, 200 grams of terpene resins, 100 grams of polyethylene wax, 5 grams of 4,4' thiobis(3-methyl-6-tert-butyl)phenol, and then Mix evenly at low speed, add to the preheated extruder hopper, set the temperature of the extruder to 130-170°C, and extrude at a screw speed of 80rpm, and the extruded product is granulated to obtain a hot melt adhesive product.
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