Recording ink as well as ink media set, ink cartridge, ink recorded matter, inkjet recording apparatus and inkjet recording method
An inkjet recording method and ink technology, applied in inks, applications, household appliances, etc., can solve the problems of low density on the back, inability to obtain images, slow drying, etc., and achieve low density on the back, good color rendering, and high image density Effect
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manufacture example 1
[0548] -Preparation of polymer solution A-
[0549]The interior of a 1 L flask equipped with a mechanical stirrer, a thermometer, a nitrogen introduction tube, a reflux tube and a dropping funnel was fully replaced with nitrogen, and then 11.2 g of styrene, 2.8 g of acrylic acid, 12.0 g of lauryl methacrylate, and 4.0 g of polyethylene were mixed. Ethylene glycol methacrylate, 4.0 g of styrene macromolecules and 0.4 g of mercaptoethanol, and the temperature was raised to 65°C. Next, 100.8 g of styrene, 25.2 g of acrylic acid, 108.0 g of lauryl methacrylate, 36.0 g of polyethylene methacrylate, 60.0 g of hydroxyethyl methacrylate, 36.0 g of A mixed solution of styrene macromolecule, 3.6 g mercaptoethanol, 2.4 g azodimethylvaleronitrile and 18 g methyl ethyl ketone. After the dropwise addition, a mixed solution of 0.8 g of azodimethylvaleronitrile and 18 g of methyl ethyl ketone was added dropwise to the flask over 0.5 hours. After aging at 65°C for 1 hour, 0.8 g of azodimethy...
manufacture example 1-1
[0551] -Preparation of Magenta Pigment Polymer Microparticle Aqueous Dispersion-
[0552] Next, 28 g of the obtained polymer solution A, 42 g of C.I. Pigment Red 122, 13.6 g of a 1 mol / L potassium hydroxide aqueous solution, 20 g of methyl ethyl ketone, and 13.6 g of ion-exchanged water were sufficiently stirred, and then kneaded with a roll mill. . The obtained slurry was put into 200 g of pure water, and after stirring sufficiently, methyl ethyl ketone and water were distilled off with an evaporator to prepare a magenta pigment polymerization of Production Example 1-1 containing 15 mass % of pigment and 20 mass % of solids. Aqueous dispersion of microparticles.
manufacture example 1-2
[0554] -Preparation of Cyan Pigment Polymer Microparticle Aqueous Dispersion-
[0555] A cyan pigment polymer fine particle aqueous dispersion of Production Example 1-2 was prepared in the same manner as in Production Example 1-1 except that C.I. Pigment Red 122 was replaced with a copper phthalocyanine pigment in Production Example 1-1. In addition, the solid content was 20 mass % and the pigment coloring agent was 12 mass % at the time of preparation.
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