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Quality control method for diabetes treating Tangniaole bolus

A quality control method and technology of Diaoxue, which are applied in the directions of pill delivery, testing of pharmaceutical preparations, measuring devices, etc., can solve problems such as the inability to effectively control the quality of preparations of Diabex, affecting product production and ensuring quality.

Inactive Publication Date: 2006-11-08
JIANGXI HUIREN PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, the existing quality control methods cannot effectively control the quality of Tang Niao Le preparations, which will affect the production and quality assurance of products.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0108] The quality control of embodiment 1 Tang Niao Le pill (concentrated pill)

[0109] The observation of traits, the steps are:

[0110] 【Properties】This product is a yellow-brown concentrated pill; slightly fragrant, pungent and slightly bitter.

[0111] Content identification, the steps are:

[0112] [Identification] (1) Take this product and observe under a microscope. The single starch grains are round, flat oval, oblong, 6-35 μm in diameter, umbilicus-shaped, herringbone-shaped, cross-shaped or short slit-shaped. , layer patterns are faintly visible. Irregular agglomerates or irregular flakes, light yellow or nearly colorless, in the form of shattered glass, with sharp edges and corners, and some visible linear textures.

[0113] (2) Take this product, grind it finely, weigh about 8g, add 50ml of chloroform, reflux for 1 hour, filter, discard the filtrate, evaporate the filter residue to dry chloroform, add 50ml of methanol to reflux for 1 hour, filter, The filtra...

Embodiment 2

[0127] Embodiment 2 Tang Niao Le Wan (concentrated pill)

[0128] 1. Prescription

[0129] Trichosanthes 104.3g Chinese yam 104.3g Astragalus 26g

[0130] Red ginseng 15.65g Rehmannia glutinosa 26g Goji berry 15.65g

[0131] Anemarrhena 15.65g Asparagus 7.8g Poria cocos 10.5g

[0132] Dogwood 10.5g Schisandra 7.8g Pueraria 10.5g

[0133] Chicken gold (fried) 10.5g

[0134] Tang Niao Le Wan (concentrated pill) preparation method:

[0135] For the above thirteen flavors, take 52.15g of yam, 52.15g of trichosanthin, gallinacea, and red ginseng, and grind them into fine powder; Add water to decoct Asparagus and Poria cocos for the first time, add 10 times the amount of water to decoct for 2 hours, add 8 times the amount of water for the second time to decoct for 2 hours, combine the decoction, filter, and concentrate the filtrate to a relative density of about 1.30 (50 ℃) thick ointment; mixed with yam, trichosanthin, gallinaceous gold, and red ginseng fine powder, made into...

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Abstract

The present invention relates to quality control method for diabetes treating Tangniaole bolus. The quality control method includes thin layer chromatography process for material identification and spectrophotometric method for content measurement. The quality control method is precise, sensitive and stable, and can ensure the high and stable product quality.

Description

Technical field: [0001] The invention relates to a quality control method for traditional Chinese medicine preparations, in particular to a quality control method for Tang Niao Le Wan (concentrated pill) preparations. Background technique: [0002] Diabetes comes from the 13th volume of the Ministry of Standards, page 225, the standard number is WS3-B-2644-97, and it is a capsule. The prescription is composed of: trichosanthum powder, yam, astragalus, red ginseng, rehmannia glutinosa, wolfberry, anemarrhena, asparagus, poria cocos, dogwood, schisandra, kudzu root, gallinacea (fried). It has the functions of nourishing yin and tonifying kidney, nourishing qi and moistening lung, harmonizing stomach and promoting body fluid, and regulating metabolism. It is used for polyphagia, polydipsia, polyuria, and weakness of limbs caused by diabetes, and reduces blood sugar and urine sugar. [0003] The pathogenesis of type 2 diabetes is related to insulin resistance and hyposecretion...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/8965A61K9/20A61K35/57A61P3/10G01N30/02G01N30/90G01N33/15
Inventor 高珍妮廖斌刘月庆耿炤
Owner JIANGXI HUIREN PHARMA CO LTD
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