Magnetic hetero nano fiber self assembling super crystal lattice structure material and its preparing method
A technology of nanofibers and structural materials, applied in nanostructure manufacturing, chemical instruments and methods, nanotechnology, etc., can solve the problems of magnetic nanofibers that have not been reported
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Embodiment 1
[0017] Embodiment 1: 0.5ml PS-b-PCEMA-b-PAA / γ-Fe 2 o 3 Put the hybrid nanofiber THF solution into a glass tube with an inner diameter of 3mm*100mm, the solution concentration is 0.08g / ml, and then put it in a 9tesla (Tesla) magnetic field. At 25°C, put the tube under the magnetic field for self-assembly Dry for 10 hours at 50°C for 8 hours. After the solvent in the glass tube evaporates to dryness, take out the glass tube, and the sample forms a film on the tube wall. After drying, the nanofiber film is peeled off from the glass tube to obtain about 0.04 g of sample. Observed under a microscope, a material with a hexagonal superlattice structure of about 20 microns can be seen.
Embodiment 2
[0018] Embodiment 2: 0.5mlPS-b-PCEMA-b-PAA / γ-Fe2 o 3 The tetrahydrofuran solution of hybrid nanofibers was put into a 5mm*150mm glass tube with a solution concentration of 0.06g / ml, placed in a 9tesla magnetic field, assembled at 25°C for 20 hours, and dried at 50°C for 10 hours. Take out the glass tube and observe it under a microscope, and you can see a material with a square superlattice structure of about 20 microns.
Embodiment 3
[0019] Embodiment 3: 0.8ml PS-b-PCEMA-b-PAA / γ-Fe 2 o 3 Put the hybrid nanofiber tetrahydrofuran solution into a 3mm*150mm glass tube with a solution concentration of 0.02g / ml, put it in a 9tesla (Tesla) magnetic field, and put the tube under the magnetic field for a period of time at 25°C, and assemble it for 18 hours After the solvent evaporates to dryness, the glass tube is taken out, and the sample forms a film on the tube wall and is dried or peeled off to obtain about 0.8 g of sample. Observed under a microscope, micron-scale cross-shaped, rod-shaped, needle-shaped superlattice structure materials can be seen.
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