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Tin-antimony oxide conducting film and its production method

A technology of oxide conduction and manufacturing method, which is applied in the direction of oxide conductors, conductive layers on insulating carriers, non-metallic conductors, etc., and can solve problems such as environmental pollution and unsuitability for industrial production

Inactive Publication Date: 2002-09-04
山东润泰智能电气有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Also have as patent application No. 99105710, its name is the manufacture method of tin dioxide transparent conductive film, although the shower nozzle is corroded relatively lightly, hydrogen chloride and / or chlorine gas can still overflow, pollute the environment, and are not suitable for industrialized production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] The tin antimony oxide conductive film comprises 85% by weight of tin dioxide and 15% by weight of antimony pentoxide, has a uniform and compact structure, a light transmittance of 80%, a resistance of 80 ohms, and a resistivity of 0.47 Ohm / cm, the thickness of the film is 110nm, and the particle size is 16nm.

[0048] The manufacturing method of described a kind of conductive film, comprises the steps in turn:

[0049] (A) Weigh 100 grams of SnCl 4 ·5H 2 O crystals, prepared into a 0.1-0.2mol / L solution with deionized water, according to Sb:SnCl 4 Weigh SbCl at an atomic ratio of 2% 3 Solid, dissolved in ethanol; stirring SnCl 4 At the same time as the solution, add an appropriate amount of citric acid to make the pH = 1.5 and then slowly add SbCl dropwise 3 alcohol solution, and heat and stir the mixed solution;

[0050] (B) When heated to 40°C, slowly add ammonia water with a concentration of 0.2mol / L until milky yellow Sn(OH) is produced 4 and Sb(OH) 3 Mix t...

Embodiment 2

[0055] The tin antimony oxide conductive film comprises 90% by weight of tin dioxide, 7% by weight of antimony pentoxide, and 3% by weight of diindium trioxide, with a uniform and compact structure and high light transmittance. It is about 85%, the resistance is 80 ohms, the resistivity is 0.47 ohms / cm, the thickness of the film is 120nm, and the particle size is 18nm.

[0056] The manufacturing method of described a kind of tin antimony oxide conductive film, comprises the following steps successively:

[0057] (A) Weigh 100 grams of SnCl 4 ·5H 2 O crystals, prepared into a 0.16mol / L solution with deionized water, according to Sb:SnCl 4 Weigh SbCl at an atomic ratio of 5% 3 Solid, according to In:SnCl 4 The number of atoms is 1% by weighing the InCl3 solid, dissolved in ethanol; stirring the SnCl 4 At the same time as the solution, add an appropriate amount of citric acid to make the pH = 2.0. Then slowly add SbCl dropwise 3 and InCl 3 alcohol solution, and heat and st...

Embodiment 3

[0063] The tin antimony oxide conductive film comprises 95% by weight of tin dioxide, 3.8% by weight of antimony pentoxide, 1.1% by weight of diindium trioxide, and 0.1% by weight of Zinc oxide has a uniform and compact structure, a light transmittance of about 85%, a resistance of 80 ohms, a resistivity of 0.47 ohms / cm, a film thickness of 120nm, and a particle size of 18nm.

[0064] Described manufacturing method is consistent with embodiment 2, and difference is added SnCl in step (A) 4 Atomic 0.1% ZnCl 2 as a resistance modifier.

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Abstract

The present invention relates to a tin-antimony oxide conducting film and its production method. Said film contains (wt%) 80%-96% of tin dioxide and 4%-20% of antimony pentoxide, their grain size diameter is 10-20 nm, and thickness is 80-180 nm. Its production method uses aqueous solution of SnCL4 and SbCL3 ethyl alcohol solution as raw material and includes the following steps: using amkmonia water to make precipitation, using oxalic acid and ammonia water to make back-solvation, concentration, preparing sol-gel, ageing, high-temp. spraying on silex glass for tin-antimony oxide conducting film with high conductivity and light transmittance, and high heat exchange efficiency.

Description

Technical field: [0001] The invention relates to the technical field of a tin antimony oxide conductive film and a manufacturing method thereof. Background technique: [0002] At present, the commonly used electric heating technology is mainly conduction in the form of electric heating wire, tin antimony oxide conductive film, etc., and diffusion heating has been widely used in many fields for decades, but there have always been problems such as slow heating speed and low thermal efficiency. Difficult to solve, and long-term use, over-current between electrodes, easy to break, peroxidation of the heating element, easy to fall off, low dielectric strength, poor heat resistance, especially for the heating of water or other liquids requires a container with a certain volume, the heating process It is easy to scale, and it is difficult to separate water or other liquids from electricity. These shortcomings make it difficult to achieve electricity safety, thus limiting its use in...

Claims

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Application Information

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IPC IPC(8): H01B1/08H01B5/14H05B3/14
Inventor 冷同桂
Owner 山东润泰智能电气有限公司
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