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Nanometer acrylic acid microemulsion, water-thinned heat reflecting and isolating paint and their production process

A nano-microemulsion and heat-insulating coating technology, which is applied in the direction of fire-proof coatings and coatings, can solve the problems of poor heat reflection and heat insulation performance, environmental pollution, etc., and achieve the goals of improving compactness, excellent heat insulation performance, and lowering temperature Effect

Inactive Publication Date: 2002-07-31
耿世斋
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved by the present invention is: the existing coatings will cause environmental pollution due to containing a large amount of organic solvents, and have poor heat reflection and heat insulation performance
[0004] In order to solve the technical problem that existing coatings will cause environmental pollution because of containing a large amount of organic solvents, the present invention adopts the following technical solutions: acrylic acid nano-microemulsion, and its special feature is: its raw material contains:

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1 to 6

[0060] As shown in Table 1, Examples 1 to 6 are the raw material ratios of six kinds of acrylic acid nano-microemulsions.

[0061]

[0062] In Table 1, benzoyl peroxide is an initiator, n-butanol is a solvent, and triethylamine, 2-amino-1-propanol and N,N dimethylethanolamine are pH regulators.

Embodiment 4

[0064] The manufacture method of the acrylic acid nano microemulsion of embodiment 4 comprises the following steps:

[0065] A. Add the first mixture of unsaturated monomers, solvents and initiators into the No. 1 reaction vessel, stir, blow nitrogen, heat up to 80-110°C, and keep warm for 1.5-2h; the first unsaturated monomer Contain methyl methacrylate, butyl acrylate, butyl methacrylate, and methacrylic acid, and their weights (g) are: 100, 200, 100, and 8; the solvent is n-butanol, and the weight is 7g; the initiator Using benzoyl peroxide, the weight is 1.0g;

[0066] B. Add the second part of the mixture of mixed unsaturated monomers, solvents and initiators into the No. 1 reaction vessel dropwise evenly. Unsaturated monomers include methyl methacrylate, butyl acrylate, butyl methacrylate, and methacrylic acid, and their weights (g) are: 75, 150, 75, and 12; the solvent is n-butanol, and the weight is 8g, initiator adopts benzoyl peroxide, weight is 0.5g;

[0067] C. ...

Embodiment 7 to 15

[0073] As shown in Table 3, Examples 7 to 15 are respectively the raw material proportions of nine kinds of water-based heat-reflecting and heat-insulating coatings.

[0074] raw material

[0075] SURFYNOL GA, dispersant 5040, dispersant Byk184, defoamer NXZ, KATHON LXE, SKANE M-8 and BCM antifungal agent in Table 3 are additives; triethylamine is PH regulator; titanium dioxide, iron oxide red , iron oxide yellow, fast yellow, phthalocyanine red and phthalocyanine blue as pigments; hollow glass microspheres and power plant floating beads as hollow microspheres; precipitated barium sulfate and fine talcum powder as fillers; self-made 1 # lotion, homemade 2 # lotion, homemade 4 # lotion and homemade 6 # The emulsions are acrylic nano-microemulsions manufactured according to the raw material formulations of the above-mentioned Examples 1, 2, 4 and 6; B-96 emulsion and AC-261 emulsion are conventional acrylic emulsions; TT-935 thickener And Rh-278 thickener as thick...

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PUM

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Abstract

The present invention is one kind of nano acrylic acid microemulsion, water-thinned heart reflecting and isolating paint with the nano acrylic acid microemulsion and their prodcution process. The present invention aims at solving the technological problems of available paint, which contains great amount of organic solvent to pollute environment and has poor heat reflecting and isoalting performance. The water-thinned heat reflecting and isolating paint consists of nano acrlic acid microemulsion, conventional acrylic acid emulsion, pigment, filler, infrared ray reflector, assistant, pH regulator, densifier and softened water. The paint contains no organic solvent and has excellent heat reflecting and isolating performance.

Description

Technical field: [0001] The invention relates to an acrylic nano-microemulsion, a water-based heat-reflecting heat-insulating coating produced by using the acrylic nano-micro-emulsion, and a manufacturing method of the acrylic nano-micro-emulsion and the water-based heat-reflecting heat-insulating coating. Background technique: [0002] Traditional coatings are mostly solvent-based, containing more than 30% organic solvents, and sometimes they are diluted with organic solvents during use. These solvents volatilize into the atmosphere during the construction process, which will not only cause harm to the health of the builders, but also pollute the environment and cause fire hazards. With the increasingly stringent environmental protection requirements around the world, it is the general trend to develop environmentally friendly coatings to replace solvent-based coatings. Ordinary coatings, especially dark-colored coatings, mostly absorb the infrared rays in sunlight and con...

Claims

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Application Information

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IPC IPC(8): C08F20/10C08F20/18C09D5/18C09D133/06C09D133/08
Inventor 耿世斋
Owner 耿世斋
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