Low-temperature sintered zinc titanate high-frequency dielectric ceramic and preparation method thereof
A technology of high-frequency dielectric and zinc titanate, which is applied in the field of high-frequency dielectric ceramics, can solve the problems of low dielectric properties of materials, high preparation costs, and complicated preparation processes, and achieve the effect of low price and reduced production cost
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Embodiment 1
[0016] In this embodiment, a chemical method is used to obtain the starting material zinc oxide for preparing the ceramic composition. The ratio of raw materials in this embodiment is: 1 part of zinc oxide produced by the decomposition of basic zinc carbonate, 1 part of nano-anatase titanium dioxide, plus 1.00% by weight of additives. The total weight of the additives is 100% of the base material.
[0017] The preparation steps are:
[0018] (1) Heat the analytically pure basic zinc carbonate to 350°C to decompose it into zinc oxide, the holding time is 3 hours, and the heating rate is 5°C / min. The particle size of the obtained zinc oxide is 50-80 nanometers.
[0019] (2) Zinc oxide and nano-anatase titanium dioxide are mixed in a molar ratio of 1: 1 and ball milled for 24 hours in a polyethylene tank with a planetary mill. With absolute ethanol and zirconium balls as the medium, the particle size of the titanium dioxide is 30-50 nanometers. The wet material after ball mill...
Embodiment 2
[0027] In this embodiment, a chemical method is used to obtain the starting material zinc oxide for preparing the ceramic composition. The ratio of raw materials in this embodiment is: 1 part of zinc oxide produced by the decomposition of basic zinc carbonate, 1 part of nano-anatase titanium dioxide, plus 1.00% by weight of additives. The total weight of the additives is 100% of the base material.
[0028] The preparation steps are:
[0029] (1) Heat the analytically pure basic zinc carbonate to 350°C to decompose it into zinc oxide, the holding time is 3 hours, and the heating rate is 5°C / min. The particle size of the obtained zinc oxide is 50-80 nanometers.
[0030] (2) Zinc oxide and nano-anatase titanium dioxide are mixed in a molar ratio of 1: 1 and ball milled for 24 hours in a polyethylene tank with a planetary mill. With absolute ethanol and zirconium balls as the medium, the particle size of the titanium dioxide is 30-50 nanometers. The wet material after ball mill...
Embodiment 3
[0038] In this embodiment, a chemical method is used to obtain the starting material zinc oxide for preparing the ceramic composition. The ratio of raw materials in this embodiment is: 1 part of zinc oxide produced by the decomposition of basic zinc carbonate, 1 part of nano-anatase titanium dioxide, plus 1.00% by weight of additives. The total weight of the additives is 100% of the base material.
[0039] The preparation steps are:
[0040] (1) Heat the analytically pure basic zinc carbonate to 350°C to decompose it into zinc oxide, the holding time is 3 hours, and the heating rate is 5°C / min. The particle size of the obtained zinc oxide is 50-80 nanometers.
[0041] (2) Zinc oxide and nano-anatase titanium dioxide are mixed in a molar ratio of 1: 1 and ball milled for 24 hours in a polyethylene tank with a planetary mill. With absolute ethanol and zirconium balls as the medium, the particle size of the titanium dioxide is 30-50 nanometers. The wet material after ball millin...
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