Cotton fiber filter disc for flue gas detection and preparation method thereof, and flue gas detection method
A flue gas detection and cotton fiber technology, applied in the field of detection and analysis, can solve the problems of interfering with the gas phase composition of flue gas components, difficult handling of fiber filters, and influence on the accurate quantification of flue gas components, so as to reduce errors, simple method and low cost cheap effect
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[0035] The invention provides a preparation method of a cotton fiber filter for smoke detection, comprising the following steps:
[0036] a) shearing natural cotton fibers to obtain broken fibers; after that, put them into a pulverizer and pulverize to obtain fine fibers;
[0037] b) dissolving the fine fibers to obtain fluffy fine fibers;
[0038] c1) get the fluffy fine fibers and make a round cake, and press by a tablet press to obtain a single-layer cotton fiber filter 1;
[0039] c2) In addition, get fluffy fine fibers to make a round cake, and press by a tablet press to obtain a single-layer cotton fiber filter 2;
[0040] c3) In addition, get fluffy fine fibers and make a round cake, and press by a tablet press to obtain a single-layer cotton fiber filter 3;
[0041] d) stacking the single-layer cotton fiber filter 1, single-layer cotton fiber filter 2 and single-layer cotton fiber filter 3, and pressing together by a tablet press to obtain a three-layer composite cot...
Embodiment 1
[0071] S1. Cut natural cotton fibers to shredded fibers with a length of 2 cm.
[0072] S2. Put the above-mentioned crushed fibers into a high-speed multifunctional pulverizer in several times, and pulverize them to fine fibers with a length of about 2 mm.
[0073] S3. Put the above-mentioned fine fibers into the SE003 standard fiber disintegrating machine, and disintegrate at 6000 rpm for 10 minutes to obtain fluffy fine fibers.
[0074] S4, take 35 mg of fluffy fine fibers, make into a round cake shape with uniform thickness, press through a tablet machine, and keep it under a pressure of 2 MPa for 10 s to obtain a single-layer cotton fiber filter 1 .
[0075] S5, take 35 mg of fluffy fine fibers, make into a round cake with uniform thickness, press through a tablet machine, and keep the pressure under 3MPa for 10s to obtain a single-layer cotton fiber filter 2.
[0076] S6, take 55 mg of fluffy fine fibers, make into a round cake with uniform thickness, press through a tab...
Embodiment 2
[0097] Example 2: Detection
[0098] 1. GC-FID quantitative analysis:
[0099] Put the filter into the filter holder, put it into a cigarette smoking device, and conduct a cigarette smoking experiment at a heating temperature of 250°C. After that, the flue gas components captured by the filter were extracted with the isopropanol solution of the internal standard (naphthalene), and the supernatant liquid was taken after 60 min of shaking extraction, filtered with a 0.45 μm organic filter membrane, and quantitatively analyzed by GC-FID.
[0100] The chromatographic setting conditions were as follows: DB-FFAP capillary column (30m×0.53mm×0.25mm), column temperature 80°C, hold for 1min, heat up to 220°C at a rate of 10°C / min, hold for 9min. The inlet temperature is 220°C, the split ratio is 2:1, and the carrier gas is H 2 , the column flow rate is 8 mL / min; the injection volume is 1 μL; the temperature of the FID detector: 260 °C.
[0101] See the results figure 1 , figure 1 ...
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