Nano inorganic gel modifier and preparation method thereof
A technology of nano-modifier and gel modifier, which is applied in the direction of cement production, etc., can solve the problems of high cost, difficulty in fire prevention and high temperature resistance of organic materials, and easy aging, etc., and achieves simple preparation method, environmental protection and green performance, low cost low effect
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Embodiment 1
[0020] A nano-inorganic gel modifier provided in the embodiment of the present invention comprises the following components in terms of weight percentage: 20-30 parts of nano-inorganic resin, 10-20 parts of nano-modifier, made of lanthanide soluble rare earth salt 4-12 parts of water-soluble rare earth water-retaining agent, 0-0.6 parts of dispersant made of inorganic airgel, 0-0.4 parts of defoamer made of water-soluble silane defoamer, and different viscosities 0-3 parts of thickener mixed with hydroxypropyl methylcellulose, 40-60 parts of deionized water, the nano-inorganic resin is fused with inorganic silicon and organic silicon under strong alkali environment at high temperature, and mixed It is prepared by chemical grafting, and the nano-modifier is made of active silicon dioxide and active aluminum oxide processed into 20-100 nanometers, and dispersed in a strong alkaline liquid according to the ratio of 2:1-5:1 ;
[0021] Using the nano-inorganic gel modifier as the ...
Embodiment 2
[0029] A kind of nanometer inorganic gel modifying agent, is prepared according to the following method:
[0030] (1) Get the following raw materials according to the weight percentage:
[0031] 30 parts of nano-inorganic resin, 15 parts of nano-modifier, 10 parts of water-soluble rare earth, 0.3 part of dispersant, 0.2 part of soluble silane defoamer, 1.5 parts of various cellulose composite thickeners, 43 parts of water;
[0032] Dissolve in the order of nano-modifiers, thickeners, inorganic resins, dispersants, and defoamers. Stir for at least 10 minutes after each addition of a raw material, and ensure that each time before adding the next material, the Stir the mixture until it is in a solution state, and stir the mixture evenly for later use after the addition is complete;
[0033] (3) Stir the mixed solution obtained in step (2) evenly, add it to a constant temperature water bath reactor, set the temperature of the reactor water bath to 65°C, adjust the stirring speed ...
Embodiment 3
[0035] A kind of nano-inorganic gel modifier provided in this embodiment is prepared according to the following method:
[0036] (1) Get the following raw materials according to the weight percentage:
[0037] 26 parts of nano-inorganic resin, 20 parts of nano-modifier, 8 parts of water-soluble rare earth, 0.3 part of dispersant, 0.2 part of soluble silane defoamer, 1.5 parts of various cellulose composite thickeners, 44 parts of water;
[0038] (2) Dissolve in the order of nano-modifier, thickener, inorganic resin, dispersant, and defoamer. Stir for no less than 10 minutes after each raw material is added, and pay attention to ensure that each raw material is added before adding the next material. Stir the mixture to a solution state at a time; after the addition is complete, stir the mixture evenly for later use;
[0039]Stir the mixed solution obtained in step (2) evenly, add it to a constant temperature water bath reactor, set the temperature of the reactor water bath to ...
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