A kind of preparation method of hydrophilic conductive polymer ultrafiltration membrane
A conductive polymer, ultrafiltration membrane technology, applied in chemical instruments and methods, membrane, membrane technology and other directions, can solve the problems of by-products, secondary pollution of the system, etc., to improve the recycling performance, oil-water separation performance and efficiency. The effect of high quantity, excellent conductivity and hydrophilicity
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Embodiment 1
[0035] Step 1. Select 316L stainless steel wire mesh, soak it in NaOH solution, use a water bath at 80°C to remove surface grease, take out the immersed stainless steel wire mesh, and rinse it with ultrapure water; the wire diameter of the 316L stainless steel wire mesh is 6-10 μm, The volume fraction of the NaOH solution was 10%, the water bath time was 1 h, and the ultrapure water was rinsed 3 times.
[0036] Step 2. Take out the stainless steel mesh in step 1 and place it in H 2 O 2 In the solution, the surface is activated with a water bath at a temperature of 80 °C to make it conducive to the electrochemical polymerization reaction, and then rinsed with ultrapure water after taking it out; to prepare the electroplating solution, a sulfuric acid solution is prepared first, and then a pyrrole solution is added to the sulfuric acid solution to prepare sulfuric acid and sulfuric acid. Mixed solution of pyrrole; H 2 O 2 The volume fraction of the solution was 2%, the water ...
Embodiment 2
[0042] Step 1. Select 316L stainless steel wire mesh, soak it in NaOH solution, use a water bath at 80°C to remove surface grease, take out the immersed stainless steel mesh, and rinse it with ultrapure water; the wire diameter of the 316L stainless steel wire mesh is 7 μm, and the NaOH solution The volume fraction is 12%, the water bath time is 1.2h, and the ultrapure water rinse is 4 times.
[0043] Step 2. Take out the stainless steel mesh in step 1 and place it in H 2 O 2 In the solution, the surface is activated with a water bath at a temperature of 80 °C to make it conducive to the electrochemical polymerization reaction, and then rinsed with ultrapure water after taking it out; to prepare the electroplating solution, a sulfuric acid solution is prepared first, and then a pyrrole solution is added to the sulfuric acid solution to prepare sulfuric acid and sulfuric acid. Mixed solution of pyrrole; H 2 O 2The volume fraction of the solution was 2.2%, the water bath time...
Embodiment 3
[0049] Step 1. Select 316L stainless steel wire mesh, soak it in NaOH solution, use a water bath at 80°C to remove surface grease, take out the immersed stainless steel mesh, and rinse it with ultrapure water; the wire diameter of the 316L stainless steel wire mesh is 9 μm, NaOH solution The volume fraction is 13%, the water bath time is 2h, and the ultrapure water rinse is 3 times.
[0050] Step 2. Take out the stainless steel mesh in step 1 and place it in H 2 O 2 In the solution, the surface is activated with a water bath at a temperature of 80 °C to make it conducive to the electrochemical polymerization reaction, and then rinsed with ultrapure water after taking it out; to prepare the electroplating solution, a sulfuric acid solution is prepared first, and then a pyrrole solution is added to the sulfuric acid solution to prepare sulfuric acid and sulfuric acid. Mixed solution of pyrrole; H 2 O 2 The volume fraction of the solution was 2.3%, the water bath time was 1 h,...
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Abstract
Description
Claims
Application Information
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