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Tantalum carbide reinforced polyether-ether-ketone composite coating and preparation method and application thereof

A technology of polyether ether ketone and composite coating, which is applied in coatings, electrolytic coatings, pharmaceutical formulations, etc., can solve problems such as insufficient mechanical strength, and achieve the effects of low price, improved wear resistance, and improved hardness

Active Publication Date: 2021-07-13
JINAN UNIVERSITY
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, when pure PEEK is used as a weighing structure in the human body, its mechanical strength is insufficient, so in order to improve its mechanical strength and osteogenic performance

Method used

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  • Tantalum carbide reinforced polyether-ether-ketone composite coating and preparation method and application thereof
  • Tantalum carbide reinforced polyether-ether-ketone composite coating and preparation method and application thereof
  • Tantalum carbide reinforced polyether-ether-ketone composite coating and preparation method and application thereof

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Embodiment Construction

[0023] The present invention will be further described in detail below with reference to the examples and drawings, but the implementation of the present invention is not limited thereto.

[0024] The reagents used in the examples can be routinely purchased from the market unless otherwise specified.

[0025] In Examples 1-11, the TaC reinforced polyetheretherketone composite coating was prepared by the following method:

[0026] (1) chitosan solution: mix 0.5g chitosan, 5mL glacial acetic acid and 500mL deionized water;

[0027] (2) Mix the above 50mL chitosan solution with 50mL ethanol evenly, then add 1-5g PEEK powder (20-30μm) and 0.01-0.2g TaC (50-100nm) to obtain a mixed solution;

[0028] (3) The mixed solution obtained in step (2) was ultrasonically dispersed for 20 minutes, stirred and dissolved for 7 hours to obtain a nano-suspension solution.

[0029] (4) Put the cathode (pure titanium) and anode (Pt) electrode materials into the nano-suspension solution obtained ...

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Abstract

The invention belongs to the technical field of biological materials and particularly discloses a tantalum carbide reinforced polyether-ether-ketone composite coating and a preparation method and application thereof. The method comprises the following steps that (1), after a chitosan solution and ethanol are uniformly mixed, PEEK powder and nanometer TaC are sequentially added in to obtain a mixed solution, and nanometer suspension liquid is obtained by ultrasonic dispersion; and (2), a cathode material and an anode material are put in the nanometer suspension liquid obtained in the step(1), direct current is introduced in, and the nanometer TaC reinforced polyether-ether-ketone composite coating is obtained through deposition. According to the tantalum carbide reinforced polyether-ether-ketone composite coating and the preparation method and application thereof, a PEEK coating is prepared on substrates of titanium and alloy thereof, stainless steel and the like through a cathode electrodeposition method, and nanometer TaC particles are introduced in a PEEK material, the osteogenesis performance of PEEK can be enhanced, and the coating prepared through cathode electrodeposition is short in production time, simple in equipment, low in price and wide in application prospect.

Description

technical field [0001] The invention belongs to the technical field of biomaterials, and in particular relates to a tantalum carbide reinforced polyetheretherketone composite coating and a preparation method and application thereof. Background technique [0002] Titanium and its alloys in artificial joint replacement materials have excellent properties, such as low density, high specific strength, good electrochemical corrosion resistance, relatively low elastic modulus and good biocompatibility. Widely used in biomedical engineering. Titanium and its alloys have the advantages of low density, high specific strength, good electrochemical corrosion resistance, low elasticity, and good biocompatibility. They are frequently used as structural components in the aerospace, automotive, petrochemical and marine industries, as well as in chemical and biomedical engineering. The main disadvantages of all titanium alloys are poor wear resistance, high coefficient of friction (COF) a...

Claims

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Application Information

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IPC IPC(8): C25D15/00A61L27/30A61L27/34A61L27/50
CPCC25D15/00A61L27/34A61L27/306A61L27/50A61L2420/02A61L2420/06A61L2430/24A61L2400/12C08L61/16
Inventor 林志丹曹琳张鹏黄素媛
Owner JINAN UNIVERSITY
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