SiOx material surface coating treatment method and device
A surface coating and slurry technology, applied in the field of lithium-ion batteries, can solve the problems of insignificant improvement in benefits, uneven coating, and difficulty in meeting mass production needs, so as to eliminate the problem of material transportation pollution and isolate the impact of the external environment. , the effect of reducing the expansion effect
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Embodiment 1
[0045] This embodiment provides a SiO x Methods of surface coating treatment of materials, including,
[0046] S1 pulping: take SiO x , Additive A, organic solvent, mix, and then perform high-speed dispersion treatment to obtain SiO x The slurry of the required particle size distribution of the particle surface coating additive A; the slurry of the required particle size distribution in this embodiment refers to SiO x The particle size is 0.2-15 μm.
[0047] S2 granulation: Atomize the slurry, heat, evaporate, and separate to obtain a granule product with the surface-coated additive A.
[0048] like figure 1 As shown, this embodiment discloses a SiO x Equipment for material surface coating treatment, including:
[0049] Slurry tank 1, for SiO x , additive A, and an organic solvent are mixed to obtain a slurry;
[0050] The high-speed dispersion device 2 is connected with the slurry tank 1, and is used for high-speed dispersion treatment of the slurry output from the slur...
Embodiment 2
[0055] like figure 1 As shown, this embodiment provides a SiO x Equipment for material surface coating treatment, including:
[0056] Slurry tank 1, for SiO x , additive A, and an organic solvent are mixed to obtain a slurry;
[0057] The high-speed dispersion device 2 is connected with the slurry tank 1, and is used for high-speed dispersion treatment of the slurry output from the slurry tank 1;
[0058] The spray drying equipment is connected with the high-speed dispersion equipment 2, and is used to spray and dry the slurry after the high-speed dispersion treatment, so as to vaporize the organic solvent in the slurry, and obtain SiO with the surface coating additive A x particles;
[0059] Cyclone separator 3, communicated with the spray drying equipment, used to separate the SiO of organic solvent gas and surface coating additive A x particles.
[0060] Further, it also includes a circulation pipeline 4, and the two ends of the circulation pipeline 4 communicate with...
Embodiment 3
[0080] The present embodiment provides a kind of SiO that adopts the device in embodiment 2 x The method of material surface coating treatment, including:
[0081] S1 pulping, take SiO x , Additive A, organic solvent, mix, and then perform high-speed dispersion treatment to obtain SiO x A slurry of the required particle size distribution of the additive A coated on the surface of the particles.
[0082] Among them, SiO x The particle size is preferably 100nm-100μm. Additive A is a long carbon chain polymer organic substance, such as monosaccharide (such as galactose, fructose, etc.), disaccharide (such as maltose, lactose, etc.), polysaccharide (such as starch, fiber One or more in element etc.); Organic solvent is alcohols, as can be one or more in ethanol, isopropanol, butanol; SiO x , Additive A, organic solvent in a weight ratio of 20:1:(50-100).
[0083] In this embodiment, the pulping process in step S1 further includes: performing a high-speed dispersion cycle on t...
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