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A kind of oral denture material and preparation method thereof

A denture and oral cavity technology, applied in the field of medical material preparation, can solve the problems of reducing elastic modulus and flexural strength, composite modification antagonism, etc.

Active Publication Date: 2022-05-10
冷高峰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Adding inorganic fillers will increase the rigidity of the material, but it will reduce its elastic modulus and flexural strength. The key to solving this contradiction is to try to choose suitable inorganic fillers or modify the inorganic fillers, and optimize the properties of modified substances and inorganic fillers. Types of inorganic fillers. At present, a single factor is used to modify a single type of inorganic filler, and compound modification often causes antagonism. Therefore, it is necessary to find an inorganic filler that can be compounded and modified to improve the rigidity of oral denture materials without reducing its elasticity. Modulus and flexural strength, is a problem to be solved urgently in this field

Method used

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  • A kind of oral denture material and preparation method thereof

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Embodiment 1

[0021] An oral denture material, the oral denture material is made of polymethyl methacrylate dispersion modified zirconia and aluminum oxide; the modified zirconia and aluminum oxide are zirconia modified by silane coupling agent and alumina; the silane coupling agent is a mixture of γ-glycidyloxypropyltrimethoxysilane and N-β-(aminoethyl)-γ-aminopropyltrimethoxysilane in a mass ratio of 1:1 mixture.

[0022] The preparation method of the above-mentioned oral denture material is carried out according to the following steps:

[0023] (1) Add the silane coupling agent into the absolute ethanol solution, configure the silane coupling agent solution with a mass concentration of 2-5%, add zirconia, alumina and hydrochloric acid aqueous solution with a mass concentration of 3-8%; The addition of zirconia accounts for 3-5% of the mass of the silane coupling agent solution; the addition of alumina accounts for 3-5% of the mass of the silane coupling agent solution; the addition of a...

Embodiment 2

[0028] An oral denture material, the oral denture material is made of polymethyl methacrylate dispersion modified zirconia and aluminum oxide; the modified zirconia and aluminum oxide are zirconia modified by silane coupling agent and alumina; the silane coupling agent is a mixture of γ-glycidyloxypropyltrimethoxysilane and N-β-(aminoethyl)-γ-aminopropyltrimethoxysilane in a mass ratio of 1:1 mixture.

[0029] The preparation method of the above-mentioned oral denture material is carried out according to the following steps:

[0030] (1) Add the silane coupling agent into the absolute ethanol solution, configure the silane coupling agent solution with a mass concentration of 2-5%, add zirconia, alumina and hydrochloric acid aqueous solution with a mass concentration of 3-8%; The addition of zirconia accounts for 3-5% of the mass of the silane coupling agent solution; the addition of alumina accounts for 3-5% of the mass of the silane coupling agent solution; the addition of a...

Embodiment 3

[0035] An oral denture material, the oral denture material is made of polymethyl methacrylate dispersion modified zirconia and aluminum oxide; the modified zirconia and aluminum oxide are zirconia modified by silane coupling agent and alumina; the silane coupling agent is a mixture of γ-glycidyloxypropyltrimethoxysilane and N-β-(aminoethyl)-γ-aminopropyltrimethoxysilane in a mass ratio of 1:1 mixture.

[0036] The preparation method of the above-mentioned oral denture material is carried out according to the following steps:

[0037] (1) Add the silane coupling agent into the absolute ethanol solution, configure the silane coupling agent solution with a mass concentration of 2-5%, add zirconia, alumina and hydrochloric acid aqueous solution with a mass concentration of 3-8%; The addition of zirconia accounts for 3-5% of the mass of the silane coupling agent solution; the addition of alumina accounts for 3-5% of the mass of the silane coupling agent solution; the addition of a...

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Abstract

The invention discloses an oral denture material and a preparation method thereof. The oral denture material is made of zirconia and aluminum oxide dispersed and modified by polymethyl methacrylate. The oral denture material of the present invention adopts modified modified zirconia and alumina as inorganic fillers, and while retaining the rigidity of the material, does not reduce its elastic modulus and flexural strength, and adopts γ-glycidyl ether oxypropyl Trimethoxysilane and N‑β‑(aminoethyl)‑γ‑aminopropyltrimethoxysilane are mixed modifiers with synergistic effect.

Description

technical field [0001] The invention belongs to the technical field of medical material preparation, and in particular relates to an oral denture material and a preparation method thereof. Background technique [0002] The development of stomatology depends on the development of materials science. Finding better oral materials has been the direction of many dental workers' efforts for many years. Dental nanocomposite is a dental restorative material composed of a resin matrix, a surface-treated inorganic filler, and an initiating system. Organic polymer is the main part of the material, which is a continuous distribution of high molecular organisms. The main function is to adhere the various components of the composite material together, giving it plasticity, curability and certain strength. It is the most commonly used restorative resin material in dentistry. Inorganic fillers in composite materials include nano-calcium carbonate, nano-silicon dioxide, nano-titanium diox...

Claims

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Application Information

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IPC IPC(8): A61K6/887A61K6/71A61K6/60
CPCA61K6/887A61K6/71A61K6/60C08L33/10
Inventor 冷高峰
Owner 冷高峰
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