Preparation method of polyurethane electronic and electrical insulating material
An insulating material, electronic and electrical technology, applied in the field of preparation of polyurethane electrical and electronic insulating materials, can solve the problems of poor applicability, general elasticity and wear resistance, corrosion resistance, poor flame retardancy, etc.
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Embodiment 1
[0018] The preparation method of the polyurethane electronic and electrical insulating material is prepared through the following steps:
[0019] Step 1: The fluorine-containing monomer molecules form an elastic polymer, using aerosol emulsion polymerization, using water as the medium, carrying the polymerization reaction and carrying the polymer evenly in it, and using low-concentration ammonium perfluorooctanoate as a dispersant to form a polymer emulsion. The polymerization reaction is carried out in the liquid phase, and the acid produced by the neutralization reaction is used as a neutralization buffer to maintain the stability of the colloid, the stability of the reaction speed and the stability of the latex concentration, and the pH is controlled at 5-6, and then (NH)S20 is used as the initiator Decompose the active group to initiate the polymerization reaction, the decomposition speed is above 85 degrees, 30% in 0.5h below 90 degrees, 50% in 1h, 75% in 2h, 90% in 3h; (N...
Embodiment 2
[0026] The preparation method of the polyurethane electronic and electrical insulating material is prepared through the following steps:
[0027]Step 1: The fluorine-containing monomer molecules form an elastic polymer, using aerosol emulsion polymerization, using water as the medium, carrying the polymerization reaction and carrying the polymer evenly in it, and using low-concentration ammonium perfluorooctanoate as a dispersant to form a polymer emulsion. The polymerization reaction is carried out in the liquid phase, and the acid produced by the neutralization reaction is used as a neutralization buffer to maintain the stability of the colloid, the stability of the reaction speed and the stability of the latex concentration, and the pH is controlled at 5-6, and then (NH)S20 is used as the initiator Decompose the active group to initiate the polymerization reaction, the decomposition speed is above 85 degrees, 30% in 0.5h below 90 degrees, 50% in 1h, 75% in 2h, 90% in 3h; (NH...
Embodiment 3
[0034] The preparation method of the polyurethane electronic and electrical insulating material is prepared through the following steps:
[0035] Step 1: The fluorine-containing monomer molecules form an elastic polymer, using aerosol emulsion polymerization, using water as the medium, carrying the polymerization reaction and carrying the polymer evenly in it, and using low-concentration ammonium perfluorooctanoate as a dispersant to form a polymer emulsion. The polymerization reaction is carried out in the liquid phase, and the acid produced by the neutralization reaction is used as a neutralization buffer to maintain the stability of the colloid, the stability of the reaction speed and the stability of the latex concentration, and the pH is controlled at 5-6, and then (NH)S20 is used as the initiator Decompose the active group to initiate the polymerization reaction, the decomposition speed is above 85 degrees, 30% in 0.5h below 90 degrees, 50% in 1h, 75% in 2h, 90% in 3h; (N...
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