Eureka AIR delivers breakthrough ideas for toughest innovation challenges, trusted by R&D personnel around the world.

High-concentration carbon nanotube slurry and preparation method thereof

A carbon nanotube, high-concentration technology, applied in chemical instruments and methods, carbon compounds, inorganic chemistry, etc., can solve problems such as poor stability of carbon nanotube slurry

Pending Publication Date: 2021-04-23
SHAANXI UNIV OF SCI & TECH
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to solve the problems in the prior art, the present invention provides a high-concentration carbon nanotube slurry and its preparation method, which solves the technical problem of poor stability of the carbon nanotube slurry in the water environment, and the preparation method is simple and easy to use. The raw material is green and pollution-free, the prepared carbon nanotube slurry can be stored stably at room temperature, and the crystal structure of the carbon nanotubes after hydrothermal treatment is not damaged

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High-concentration carbon nanotube slurry and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0022] The invention provides a kind of preparation method of high-concentration carbon nanotube slurry, comprising the following steps:

[0023] 1) Mix carbon nanotube powder and ionic liquid crystal with a mass ratio of (1:1) to (5:1) and add them into deionized water, stir and mix well to obtain a mixed solution; preferably, the particle size of the carbon nanotube powder 2-5nm; ionic liquid crystals include imidazole ionic liquid crystals; further preferably, ionic liquid crystals include 1-hexadecyl-3-methylimidazole bromide, 1-hexadecyl-3-methylimidazolium tetrafluoroboron salt, 1-hexadecyl-3-methylimidazole hexafluorophosphate, 1-dodecyl-3-methylimidazole chloride and 1-dodecyl-3-methylimidazole bromide One or more of them; the concentration of ionic liquid crystal is 2.5-20mg / mL; the amount of deionized water is 10-30ml, and the mass ratio of deionized water to carbon nanotube powder is (10:1)~(30:1 );

[0024] 2) Put the mixed solution in a reaction kettle, and cond...

Embodiment 1

[0029] (1) Weigh 1-hexadecyl-3-methylimidazole bromide and carbon nanotube powder with a mass ratio of 1:2 and add them into 30ml deionized water, stir vigorously until fully dissolved in deionized water, and obtain Mixed solution of carbon nanotube powder and ionic liquid crystal;

[0030] (2) Add the homogeneously mixed mixed solution into a polytetrafluoroethylene-lined reaction kettle, and perform a high-temperature hydrothermal reaction at 180° C. for 12 hours;

[0031] (3) Pour out the product after the hydrothermal reaction to obtain a high-concentration carbon nanotube slurry.

Embodiment 2

[0033] (1) Weigh 1-hexadecyl-3-methylimidazolium tetrafluoroborate and carbon nanotube powder with a mass ratio of 1:3 and add them to 30mL deionized water, stir vigorously until fully dissolved in deionized water, Obtain a mixed solution for carbon nanotube powder and ionic liquid crystal;

[0034] (2) Add the homogeneously mixed mixed solution into a polytetrafluoroethylene-lined reaction kettle, and perform a high-temperature hydrothermal reaction at 180° C. for 15 hours;

[0035] (3) Pour out the product after the hydrothermal reaction to obtain a high-concentration carbon nanotube slurry.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a high-concentration carbon nanotube slurry and a preparation method thereof, and solves the technical problem of poor stability of the carbon nanotube slurry in a water environment, the preparation method comprises the following steps: 1) mixing carbon nanotube powder and ionic liquid crystal in a mass ratio of (1: 1)-(5: 1), adding the mixture into deionized water, and fully stirring and uniformly mixing to obtain a mixed solution; 2) putting the mixed solution into a reaction kettle, and carrying out hydrothermal reaction at 150-250 DEG C; 3) taking out a product after the hydrothermal reaction to obtain high-concentration carbon nanotube slurry; the prepared high-concentration carbon nanotube slurry is high in concentration and good in dispersity, can be stably stored for more than 6 months for a long time under the condition of normal temperature, and has relatively high application value.

Description

technical field [0001] The invention relates to the technical field of carbon nanotube slurry preparation, in particular to a high-concentration carbon nanotube slurry and a preparation method thereof. Background technique [0002] Carbon nanotubes are seamless concentric nanoscale tube structures formed by curling graphite sheets, and hemispherical large fullerene molecules formed by five-membered rings and seven-membered rings seal both ends, in which carbon is sp 2 bonded by hybridization. According to the number of layers of graphite sheets in the tube, it can be divided into single-walled carbon nanotubes and multi-walled carbon nanotubes. The extremely high aspect ratio and super strong mechanical properties make carbon nanotubes a one-dimensional nanomaterial with high application potential. Its applications have involved nanoelectronic devices, catalyst supports, electrochemical materials, hydrogen storage materials and composite material enhancements. In many ways...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C01B32/174
CPCC01B32/174
Inventor 宋浩杰兰梦田瑞贾晓华杨进李永王思哲
Owner SHAANXI UNIV OF SCI & TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com