Transparent fireproof glue, preparation method thereof and composite fireproof glass containing transparent fireproof glue
A technology of fireproof glass and fireproof glue, applied in the field of fireproof glue, can solve the problems of difficult application, easy generation of micro-bubbles, poor ultraviolet radiation resistance and high temperature resistance, etc., to prevent heat conduction and radiation, and low temperature resistance. Improved performance and the effect of preventing the spread of flames
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[0076] One embodiment of the present invention also proposes a preparation method of transparent fireproof glue, which specifically includes the following steps:
[0077]Add char-forming agent, char-forming aid, heat-resistant stabilizer, inorganic anti-condensation agent, ion fixative, storage stabilizer, defoamer and cross-linking agent in sequence to the nano-silica sol, and stir while adding. After being uniform, the first solution is obtained;
[0078] Add the water glass solution to the first solution, or add the first solution to the potassium water glass solution, transfer to a vacuum stirring tank, control the temperature of the system within 60°C, preferably 20-60°C, and stir for 30-60min, Then degas under a vacuum lower than -0.096MPa for 30-40min, and after pressure relief, filter the solution with a 150-200 mesh screen to obtain a transparent fireproof glue;
[0079] Wherein, the raw materials in this method are the same as those of the aforementioned transparent...
Embodiment 1
[0122] A kind of transparent fireproof glue, it is made of the following raw materials in parts by weight: 50 kg of nano-silica sol with a mass concentration of 45%, 38 kg of potassium water glass solution with a mass concentration of 40%, 0.5 kg of sucrose, and dihydrogen phosphate Potassium 0.1kg, boric acid 0.3kg, glycerol 5kg, MgCl 2 10kg, starch 0.05kg, sodium polyphosphate 0.4kg, polyether modified silicone 0.5kg and sodium fluorosilicate 0.15kg.
[0123] The preparation method of the transparent fireproof adhesive specifically includes the following steps: sequentially adding a char-forming agent, a char-forming auxiliary agent, a heat-resistant stabilizer, an inorganic anti-condensation agent, an ion fixative, a storage stabilizer, and a defoaming agent to the nano-silica sol. agent and cross-linking agent, stir evenly to obtain the first solution; mix the potassium water glass solution with the first solution, stir at a temperature of 40°C for 50min, and degas under ...
Embodiment 2
[0138] A kind of transparent fireproof glue, and it is made of following raw material in parts by weight: 55kg of nano-silica sol with a mass concentration of 48%, 28kg of sodium water glass solution with a mass concentration of 42%, 0.3kg of fructose, and potassium hydrogen phosphate 0.2kg, borax 0.5kg, ethylene glycol 2kg, MgCl 2 13kg, zinc oxide 0.1kg, potassium polyphosphate 0.5kg, polyoxyethylene polyoxypropylene pentaerythritol ether 0.2kg and aluminum fluoride 0.3kg.
[0139] The preparation method of the transparent fireproof adhesive specifically includes the following steps: sequentially adding a char-forming agent, a char-forming auxiliary agent, a heat-resistant stabilizer, an inorganic anti-condensation agent, an ion fixative, a storage stabilizer, and a defoaming agent to the nano-silica sol. agent and cross-linking agent, stir evenly to obtain the first solution; mix the potassium water glass solution with the first solution, stir at a temperature of 60°C for 3...
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