Industrial heat-resistant silane modified polyether sealant and preparation method thereof
A silane-modified polyether and sealant technology, applied in the direction of polyether adhesives, adhesives, adhesive types, etc., can solve problems such as poor heat resistance, ensure heat resistance and paintability, and improve heat resistance. performance and durability, and the effect of meeting the requirements of process adhesive spraying
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Embodiment 1
[0043] 85 parts of silane-modified polyether with a number average molecular weight of 14274, 50 parts of polypropylene glycol PPG3000, 10 parts of diisodecyl phthalate, 120 parts of nanometer calcium carbonate, 50 parts of heavy calcium carbonate, 10 parts of kaolin, 6 Part specific surface area is 150m 2 Add / g of fumed white carbon black into the high-speed disperser, stir at a low speed for 20 minutes until uniform, then raise the temperature of the material to 110°C and stir for 2 hours under a vacuum of -0.085MPa to obtain a mixed material; when the temperature of the mixed material is lowered to below 45°C, Add 3 parts of carbon black slurry, 5.5 parts of oligomer vinyltrimethoxysilane, 1.5 parts of benzotriazole UV absorber, 1.5 parts of hindered amine light stabilizer, 3 parts of N-β-(aminoethyl) -γ-Aminopropyltrimethoxysilane, 0.5 part of γ-(2,3-glycidoxy)propyltrimethoxysilane, 0.7 part of dibutyltin dilaurate, stirred at -0.085MPa vacuum for 40min and discharged ,...
Embodiment 2
[0045] 96 parts of silane-modified polyether with a number average molecular weight of 10012, 40 parts of diisononyl phthalate, 100 parts of nano-calcium carbonate, 40 parts of kaolin, 20 parts of silicon micropowder, 5 parts of titanium dioxide, and 2 parts of polyamide Add the wax into the high-speed disperser, stir at a low speed for 20 minutes until uniform, then raise the temperature of the material to 110°C and stir for 2 hours under a vacuum of -0.085MPa to obtain a mixed material; when the temperature of the mixed material is cooled below 45°C, add 6.7 parts of vinyl trimethoxy base silane, 1 part of salicylate UV absorber, 1 part of hindered amine light stabilizer, 4.2 parts of γ-aminopropyl trimethoxysilane, 0.2 part of chelated tin, and stirred for 40 minutes under -0.085MPa vacuum. material, to obtain the industrial heat-resistant silane-modified polyether sealant of the present invention.
Embodiment 3
[0047]98 parts of silane-modified polyether with a number average molecular weight of 23500, 75 parts of polypropylene glycol PPG3000, 128 parts of nano-calcium carbonate, 64 parts of heavy calcium carbonate, and 7 parts with a specific surface area of 150m 2 Add / g of fumed white carbon black into the high-speed disperser, stir at a low speed for 20 minutes until uniform, then raise the temperature of the material to 110°C and stir for 2 hours under a vacuum of -0.085MPa to obtain a mixed material; when the temperature of the mixed material is lowered to below 45°C, Add 5 parts of oligomer vinyltrimethoxysilane, 2 parts of benzophenone UV absorber, 2 parts of hindered amine light stabilizer, 3.6 parts of γ-aminopropyl triethoxysilane, 1.8 parts of γ-(2 , 3-glycidoxy)propyltrimethoxysilane and 0.8 parts of stannous octoate were stirred under a vacuum of -0.085 MPa for 40 minutes and then discharged to obtain the industrial heat-resistant silane-modified polyether sealant of t...
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