Method for preparing xylooligosaccharide from corn bran
A technology of xylooligosaccharides and corn husks, which is applied in the preparation of oligosaccharides and sugar derivatives, chemical instruments and methods, etc. It can solve the problems of poor recovery of waste heat steam, large sewage discharge, and low light transmittance of feed liquid, etc. problems, to achieve the effect of reducing acid and alkali consumption, reducing the amount of sewage, and convenient recovery of waste heat
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Embodiment 1
[0034] A method for preparing xylooligosaccharides from corn bran, comprising the following steps:
[0035] (1) First in the syrup tank (full volume 25m 3 ) Riga process water 18m 3 , then add 2t of corn bran (water content<12%), add acid to adjust the pH to 4.5, heat up to 80°C, stir and mix evenly; obtain the suspension of corn bran; in the present embodiment, the acid added is acetic acid, add Other acids will affect the purity of xylo-oligosaccharides after enzymatic hydrolysis. Corn husks can be purchased commercially. The moisture content of the corn hulls is 10%, and the ash content is lower than 2%. In this embodiment, the ash content is 1%.
[0036] (2) Start the conveying pump, deliver the suspension of corn bran obtained in step (1) to the booster injector, open the steam valve of the booster injector simultaneously, steam heat the material, and ensure that the steam pressure of the injector is at 0.6 MPa, keep the temperature of the material at 160°C, then tran...
Embodiment 2
[0048] A method for preparing xylooligosaccharides from corn bran, comprising the following steps:
[0049] (1) First in the syrup tank (full volume 25m 3 ), then add corn bran (water content<12%), the mass ratio of corn bran to water is 1:9, add acid to adjust pH to 5, heat up to 85°C, stir and mix evenly; obtain corn bran Suspension: In this embodiment, the acid added is acetic acid, adding other acids will affect the purity of xylo-oligosaccharides after enzymatic hydrolysis. Corn husks can be purchased commercially. The moisture content of corn hulls is 8%, and the ash content is lower than 2%. In this embodiment, the ash content is 0.5%.
[0050] (2) Start the conveying pump, convey the suspension of corn husks obtained in step (1) to the booster injector, open the steam valve of the booster injector at the same time, steam heat the material, and then transport the material to the laminar flow tank , to ensure that the vapor pressure of the ejector is at 0.7MPa, to kee...
Embodiment 3
[0063] A method for preparing xylooligosaccharides from corn bran, comprising the following steps:
[0064] (1) First in the syrup tank (full volume 25m 3 ), then add corn bran (water content<12%), the mass ratio of corn bran to water is 1:10, add acid to adjust pH to 5.5, heat up to 90°C, stir and mix evenly; obtain corn bran Suspension: In this embodiment, the acid added is acetic acid, adding other acids will affect the purity of xylo-oligosaccharides after enzymatic hydrolysis. Corn husks can be purchased commercially. The moisture content of the corn hulls is 5%, and the ash content is lower than 2%. In this embodiment, the ash content is 0.5%.
[0065] (2) Start the conveying pump, convey the suspension of corn husks obtained in step (1) to the booster injector, open the steam valve of the booster injector at the same time, steam heat the material, and then transport the material to the laminar flow tank , ensure that the vapor pressure of the ejector is at 0.7MPa, ke...
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