Method for synthesizing olefin by electro-catalyzing semi-hydrogenated gas-phase alkyne
A hydrogenation gas, electrocatalysis technology, applied in electrodes, electrolysis process, electrolysis components, etc., can solve the problems of low current density and alkyne conversion rate, not receiving attention from researchers, and achieve the improvement of current density and alkynes. Conversion, effect of excellent olefin selectivity
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Embodiment 1
[0055] (1) The gas diffusion electrode made of Fe nanoparticles is used as the cathode of the electrolytic cell; the gas diffusion electrode made of iridium oxide catalyst is used as the anode of the electrolytic cell; both the catholyte and the anolyte are 1M KOH solution, and an anion is used between exchange membrane isolation, and as figure 1 The schematic diagram of the apparatus shown assembles the various components.
[0056] (2) Use a gas mass flowmeter to control the flow rate of the acetylene reaction gas to 50 sccm.
[0057] (3) A peristaltic pump is used to control the flow rate of catholyte and anolyte to 50 sccm.
[0058] (4) The catalytic activity of Fe nanoparticles was characterized by potentiostatic method.
[0059] The catalyst composition and specific evaluation results are shown in Table 1.
Embodiment 2
[0061] (1) The gas diffusion electrode made of Co nanoparticles is used as the cathode of the electrolytic cell; the gas diffusion electrode made of iridium oxide catalyst is used as the anode of the electrolytic cell; both the catholyte and the anolyte are 1M KOH solution, and anion is used between exchange membrane isolation, and as figure 1 The schematic diagram of the apparatus shown assembles the various components.
[0062] (2) Use a gas mass flowmeter to control the flow rate of the acetylene reaction gas to 50 sccm.
[0063] (3) A peristaltic pump is used to control the flow rate of catholyte and anolyte to 50 sccm.
[0064] (4) The catalytic activity of Co nanoparticles was characterized by potentiostatic method.
[0065] The catalyst composition and specific evaluation results are shown in Table 1.
Embodiment 3
[0067] (1) The gas diffusion electrode made of Ni nanoparticles is used as the cathode of the electrolytic cell; the gas diffusion electrode made of iridium oxide catalyst is used as the anode of the electrolytic cell; both the catholyte and the anolyte are 1M KOH solution, and an anion is used between exchange membrane isolation, and as figure 1 The schematic diagram of the apparatus shown assembles the various components.
[0068] (2) Use a gas mass flowmeter to control the flow rate of the acetylene reaction gas to 50 sccm.
[0069] (3) A peristaltic pump is used to control the flow rate of catholyte and anolyte to 50 sccm.
[0070] (4) The catalytic activity of Ni nanoparticles was characterized by potentiostatic method.
[0071] The catalyst composition and specific evaluation results are shown in Table 1.
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