Fumigation insecticide, preparation method of fumigation insecticide and disinfection and killing method adopting fumigation insecticide

An insecticide, chlorantraniliprole technology, applied in the field of insecticides, can solve problems such as waste, low phosphine concentration, and fast decay of phosphine concentration, so as to reduce costs, improve safety, and improve thermal stability Effects on Sexuality and Chemical Stability

Inactive Publication Date: 2021-01-19
河南省紫风养护发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the process of insect control and insecticide in the warehouse, if the amount of aluminum phosphide is low, the concentration of phosphine produced by the decomposition of aluminum phosphide will be low, and the concentration of phosphine will decay quickly, so it cannot play the role of insecticide for a long time. Function; if the amount of aluminum phosphide is high, the cost of insect control and insecticide will increase, resulting in waste

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example

[0060] In the following preparation examples, examples and comparative examples:

[0061] Cyhalothrin was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.;

[0062] Chlorantraniliprole was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.;

[0063] DMC catalyst was purchased from Changzhou Hongyu Chemical Co., Ltd.;

[0064] 1,4-Dioxane was purchased from Jinan Hongquan Titanium Industry Co., Ltd.

preparation example 1

[0066] Castor oil polyether polyol adopts following method to make:

[0067] Mix 166g of castor oil and a catalytic amount of DMC catalyst, replace it with nitrogen for 3 times, then raise the temperature to 115°C, vacuum dehydrate, then add 334g of epoxide (propylene oxide 184g , epoxycyclohexane 150g), reacted for 30 minutes, vacuum degassed for 30 minutes, and then filtered at a temperature of 60°C to obtain castor oil polyether polyol.

preparation example 2

[0069] Castor oil polyether polyol adopts following method to make:

[0070] Mix 167g of castor oil and a catalytic amount of DMC catalyst, replace it with argon three times, then raise the temperature to 120°C, vacuum dehydrate, then add 336g of epoxide (propylene oxide) at a temperature of 145°C and a pressure of 0.3MPa 184.5g, epoxycyclohexane 151.5g), reacted for 35min, vacuum degassed for 35min, and then filtered at a temperature of 62.5°C to obtain castor oil polyether polyol.

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PUM

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Abstract

The invention relates to a fumigating insecticide, a preparation method of the fumigating insecticide and a disinfection and killing method adopting the fumigating insecticide. The fumigating insecticide is prepared from the following components in parts by weight: aluminum phosphide, cyhalothrin, chlorantraniliprole, ethanol, polyethylene glycol, phenolic resin, guar gum, calcium alginate and castor oil polyether polyol. The preparation method of the fumigating insecticide comprises the following steps: mixing and stirring all the raw materials at the temperature of 55-65 DEG C, then rapidlycondensing, and drying at the temperature of 40-50 DEG C to obtain the fumigating insecticide. The disinfecting and killing method adopting the fumigating insecticide comprises the following steps: atthe temperature of 20-25 DEG C and the humidity of 30-33RH%, putting the fumigating insecticide into a closed space at the usage amount of 6-10g / m < 3 >; the fumigating insecticide has the effect ofstably and durably releasing hydrogen phosphide, so that the effect of durably preventing and killing insects can be achieved by using a relatively small amount of fumigating insecticide, and the costof the disinfecting and killing process is saved.

Description

technical field [0001] The present application relates to the technical field of pesticides, in particular to a fumigating pesticide, a preparation method thereof and a disinfecting method using the pesticide. Background technique [0002] Tobacco leaves, as raw materials for the tobacco industry, are generally stored in warehouses for a long time, and tobacco leaves generally contain basic nutrients needed for the growth of microorganisms and insects, such as glucose, protein, organic acids, chlorophyll, nicotine, etc. Therefore, tobacco leaves In the process of long-term storage in the warehouse, pests are more likely to occur. Tobacco leaves infested by pests will be mildewed, broken, perforated, and the yield of silk will decrease. In addition, insect eggs, insect excrement, insect corpses, etc. will also pollute the tobacco leaves, affecting the quality of the tobacco leaves, and more seriously will make the tobacco leaves unusable. value. Therefore, during the storag...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N59/26A01N53/08A01N43/56A01N25/10A01N25/18A01N25/22A01P7/04
CPCA01N25/10A01N25/18A01N25/22A01N43/56A01N53/00A01N59/26
Inventor 刘家辛
Owner 河南省紫风养护发展有限公司
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