Preparation method of plant antibacterial, antiviral, skin-care and health-care cellulose fibers
A technology of cellulose fiber and cellulose A, applied in the direction of cellulose/protein conjugated rayon, cellulose/protein rayon chemical post-treatment, fiber chemical characteristics, etc., can solve the problem of affecting the functionality of fibers or fabrics , loss, easy loss and other problems, to achieve the effect of good skin care and health care functions
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Embodiment 1
[0044] A preparation method of plant-based antibacterial, antiviral, skin care and health care cellulose fiber whose specification is 1.33dtex*38mm is as follows:
[0045] 1. Preparation of collagen solution
[0046] Prepare a 2.0mol / L urea solution, add collagen with a molecular weight of 110kD to the prepared urea solution at a mass fraction of 8.0%, and dissolve at 85°C for 1.5h to obtain collagen with a falling ball viscosity of 15s lysate.
[0047] 2. Preparation of tea polyphenol dispersion
[0048] Tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) were added to deionized water at 35°C and pH=7, stirred and dissolved for 30 minutes to prepare a tea polyphenols dispersion with a mass fraction of 10% tea polyphenols.
[0049] 3. Preparation of blended spinning stock solution
[0050] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. The dissolving solution i...
Embodiment 2
[0057] A preparation method of plant-based antibacterial, antiviral, skin care and health care cellulose fibers with a specification of 1.56dtex*38mm is as follows:
[0058] 1. Preparation of collagen solution
[0059] Prepare a 2.8mol / L urea solution, add collagen with a molecular weight of 175kD to the prepared urea solution at a mass fraction of 10.5%, and dissolve at 82°C for 2.0h to obtain collagen with a falling ball viscosity of 21s lysate.
[0060] 2. Preparation of tea polyphenol dispersion
[0061] Add tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) into deionized water at 41°C and pH=7, start stirring and dissolving for 39 minutes, and prepare a tea polyphenol dispersion with a mass fraction of 12.5% tea polyphenols.
[0062] 3. Preparation of blended spinning stock solution
[0063] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. The dissolving...
Embodiment 3
[0070] A kind of preparation method of plant antibacterial antiviral, skin care and health care cellulose fiber whose specification is 1.67dtex*38mm is as follows:
[0071] 1. Preparation of collagen solution
[0072] Prepare a 3.5mol / L urea solution, add collagen with a molecular weight of 235kD to the prepared urea solution at a mass fraction of 12.6%, heat up to 76°C and dissolve for 2.5h to obtain collagen with a falling ball viscosity of 25s lysate.
[0073] 2. Preparation of tea polyphenol dispersion
[0074] Tea polyphenols (purchased from Xi'an Zelang Biotechnology Co., Ltd.) were added to deionized water at 46°C and pH=7, stirred and dissolved for 43 minutes, and a tea polyphenol dispersion with a mass fraction of 15.6% of tea polyphenols was prepared.
[0075] 3. Preparation of blended spinning stock solution
[0076] Using cellulose pulp as raw material, the cellulose spinning stock solution was prepared through the conventional viscose preparation process. Its c...
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