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Solder wire soldering flux capable of reducing splashing and preparation method thereof

A flux and solder wire technology, applied in welding equipment, welding media, manufacturing tools, etc., can solve problems such as inability to suppress bubble splash, reduce solder joint reliability, and environmental hazards, so as to improve solder joint reliability and suppress spatter , Improve the effect of soldering performance

Active Publication Date: 2020-11-10
云南锡业新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when the solder wire is soldered at high temperature, the flux will always melt and boil, decompose to generate a relatively high-pressure air pressure, and form a certain amount of high-pressure bubbles. The bursting of the bubbles will cause considerable splashes. Although the above prior art effectively reduces the Splash, but it cannot suppress the splash caused by bubble burst. In addition, fluorine-containing surfactants and ionic surfactants are used in the flux formula, which will bring certain harm to the environment and reduce the reliability of solder joints.

Method used

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  • Solder wire soldering flux capable of reducing splashing and preparation method thereof
  • Solder wire soldering flux capable of reducing splashing and preparation method thereof
  • Solder wire soldering flux capable of reducing splashing and preparation method thereof

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Embodiment 1

[0036] A solder wire flux that can reduce spatter, its composition and mass percentage are:

[0037]

[0038] The preparation method of solder wire flux that can reduce spatter is as follows: Add hydrogenated rosin and modified rosin R130 into the reactor, heat to 155°C, stir and melt completely, and keep the temperature at about 145°C, then add glutaric acid, decane Diacid, dodecanedioic acid and dibromobutenediol were stirred for 5-10 minutes to melt completely to obtain a composite compound; tetrahydrofurfuryl alcohol and propylene glycol monomethyl ether were mixed to obtain a compound solvent, and p-tert-butyl Add imidazole hydrobromide, Ciba antioxidant 1010, and benzotriazole into the compound solvent and stir fully to obtain a compound solution; then add the compound ingredients into the compound solution and stir at constant temperature for 1-5 minutes, and finally add Surfynol 104BC, Dynol 604, methyl silicone oil, silicone defoamer, continue to stir for 20 minute...

Embodiment 2

[0041] A solder wire flux that can reduce spatter, its composition and mass percentage are:

[0042]

[0043] The preparation method of solder wire flux that can reduce spatter is as follows: add hydrogenated rosin, Eastman fully hydrogenated rosin AX-E, and modified rosin RHR-604B into the reactor and heat to 160 ° C to stir and melt completely, and keep the temperature at 150 At about ℃, add phenylbutanedioic acid, sebacic acid and dibromobutenediol at the same time, stir for 5-10 minutes to melt completely, then add cyclohexylamine hydrobromide, p-tert-butyl In the compound solvent of imidazole hydrobromide, Ciba antioxidant 1010, and benzotriazole (the compound solvent is compounded by ethanolamine, propylene glycol monomethyl ether, and tripropylene glycol butyl ether), stir at constant temperature for 1-5 minutes, Finally, add the mixture of DF110D and silicone defoamer, and continue to stir for 20 minutes to completely dissolve the components and mix well to prepare ...

Embodiment 3

[0046] A solder wire flux that can reduce spatter, its composition and mass percentage are:

[0047]

[0048]

[0049] The preparation method of the solder wire flux that can reduce spatter is as follows: Add water white rosin, Eastman fully hydrogenated rosin AX-E, modified rosin RHR-604B, and hydrogenated rosin into the reactor and heat to 165 ° C to stir and melt completely. And keep the temperature at about 160°C, then add adipic acid, sebacic acid and dibromobutene diol at the same time, stir for 5-10 minutes to make it melt completely, then add diethylamine hydrobromide dissolved in it, In the compound solvent of tert-butyl imidazole hydrobromide, Ciba antioxidant 1010, and imidazole (the compound solvent is compounded by diethylene glycol, dipropylene glycol butyl ether, methanol, and tripropylene glycol monomethyl ether), Stir at constant temperature for 1-5 minutes, finally add the mixture of SurfynolAD01, Surfynol 104E, and methyl silicone oil, and continue to ...

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Abstract

The invention relates to a solder wire soldering flux capable of reducing splashing and a preparation method thereof. The soldering flux is composed of the following components in percentage by weightof 1.0-10.0% of compound organic acid, 0.2-5.0% of compound activator, 0.1-1.0% of compound defoamer, 2.0-10.0% of compound solvent, 0.1-1.0% of antioxidant, 0.1-1.0% of corrosion inhibitor and the balance of compound rosin. The preparation method comprises the following steps of heating, stirring and melting the compound rosin, adding the compound organic acid and the low-melting-point indissolvable activator, adding the solution dissolved with the high-melting-point dissolvable activator, the antioxidant and the corrosion inhibitor, finally adding the compound defoamer, performing continuous stirring at the constant temperature of 145-165 DEG C, performing full dissolving, and performing uniform mixing, thereby obtaining the soldering flux. The soldering flux is high in activity, easy to tin during welding, low in corrosion, small in residue and high in insulation resistance, the splashing number and the splashing distance of the soldering flux and tin beads in the welding process of a lead-free tin wire can be greatly reduced, the RoHS instruction is met, and the reliability of electronic and electrical products after welding is guaranteed.

Description

technical field [0001] The invention belongs to the technical field of electronic soldering materials, and in particular relates to a solder wire flux and a preparation method thereof. Background technique [0002] With the rapid development of electronic information products, the welding requirements for solder wire are getting higher and higher. Among them, the performance of splashing and frying tin is one of the important indicators for evaluating the quality level of a solder wire. It directly affects the quality of electronic products and will Harm to the health of welding workers. Therefore, many standards have incorporated the splash test into the testing items, such as the international standard IPC-TM-650, IPC J-STD-004B, etc. Although the national standard does not include the splash test as a testing item, most domestic manufacturers have included it Splash test is one of the important criteria for solder wire quality evaluation. [0003] In this regard, domest...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23K35/363B23K35/40
CPCB23K35/3612B23K35/3613B23K35/3618B23K35/40
Inventor 何江华白海龙张欣吕金梅赵玲彦解秋莉沙文吉徐浩雷佳熙
Owner 云南锡业新材料有限公司
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