Ternary positive electrode material precursor with specific morphology and preparation method thereof
A technology of positive electrode material and precursor, applied in the field of ternary positive electrode material precursor and its preparation, can solve the problems that affect the processing performance such as sintering, do not involve primary particles, and do not fully elaborate, so as to save washing cost and size Uniformity and the effect of reducing the number of washings
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Embodiment 1
[0036] A ternary cathode material precursor with specific morphology, the molecular formula is Ni 0.65 co 0.07 mn 0.28 (OH) 2 :D 0 =1.63um,D 10 =2.76um, D 50 =3.85um,D 90 =5.37um,D 100 =8.6um; the average particle size of the primary particles of this type of precursor is 200-300nm, and the secondary particles are formed by the agglomeration of lath-shaped primary particles. Tap density 2.02g / cm 3 , specific surface area 10m 2 / g, bulk density 1.47g / cm 3 , Na content 73ppm. Spherical or spherical.
[0037] The preparation method of the above-mentioned ternary positive electrode material precursor with specific morphology comprises the following steps:
[0038] S1: According to Ni 0.65 co 0.07 mn 0.28 (OH) 2 The molar ratio of metal elements in the chemical formula prepares the soluble mixed salt solution that the molar concentration of metal ions is 1.6mol / L, and the solvent is water; prepare 32% sodium hydroxide solution and 22% ammonia solution at the same ti...
Embodiment 2
[0051] A ternary cathode material precursor with specific morphology, the molecular formula is Ni 0.52 co 0.20 mn 0.28 (OH) 2 :D 0 =2.39um,D 10 =6.547um, D 50 =10.12um,D 90 =16.39um,D 100 =31.05um; the average particle size of the primary particles of this type of precursor is 200-300nm, and the secondary particles are formed by the agglomeration of lath-shaped primary particles. Tap density 2.34g / cm 3 , specific surface area 8m 2 / g, bulk density 1.9g / cm 3 , Na content 80ppm. Spherical or spherical.
[0052] The preparation method of the above-mentioned ternary positive electrode material precursor with specific morphology comprises the following steps:
[0053] S1: According to Ni 0.52 co 0.20 mn 0.28 (OH) 2 The molar ratio of metal elements in the chemical formula prepares the soluble mixed salt solution that the molar concentration of metal ions is 2.0mol / L, and the solvent is water; prepare 32% sodium hydroxide solution and 22% ammonia solution at the same...
Embodiment 3
[0065] Example 3 is basically the same as Example 1, except that in step S2, the ammonia concentration is controlled at 6.5 g / L, and then sodium hydroxide solution is added to adjust the pH of the mixture to 11.3-11.5.
[0066] The appearance of the product obtained in Example 3 is substantially the same as that of the product in Example 2, and will not be repeated here.
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