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Oil slurry scale inhibitor of catalytic cracking unit and preparation method thereof

A technology for catalytic cracking unit and scale inhibitor, which is used in the petroleum industry, hydrocarbon oil treatment, and treatment equipment corrosion/fouling inhibition, etc., can solve the problems of lowering the temperature at the bottom of the tower, lowering the heat exchange effect, and increasing the yield of oil slurry, etc. To achieve the effect of enhanced anti-corrosion performance, good dispersion, simple and easy-to-control process

Pending Publication Date: 2020-07-10
北京乐文科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It will cause unplanned shutdown, but the heat exchange effect of the oil slurry heat exchanger is reduced due to fouling, and the return refining oil (quench oil) is injected into the bottom of the tower to reduce the temperature at the bottom of the tower, and the heat extraction requirement is met by reducing the pressure of the steam drum, causing the fractionation tower The operating flexibility is very small, the product distribution becomes poor, and the oil slurry yield increases, which seriously limits the processing capacity of the fractionation tower, seriously affecting the safety and long-term operation of the device
[0004] However, there is currently no effective solution to these fouling situations.

Method used

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  • Oil slurry scale inhibitor of catalytic cracking unit and preparation method thereof
  • Oil slurry scale inhibitor of catalytic cracking unit and preparation method thereof

Examples

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Effect test

Embodiment 1

[0027] This embodiment provides a kind of preparation method of the oil slurry antiscalant of catalytic cracking unit:

[0028] 5kg N-cyclohexylthiophthalamide, 5kg 2-tert-butyl hydroquinone, 25kg sodium dodecyl sulfate, 5kg oleylamine ethyl imidazoline, 15kg xylene and 45kg 200# solvent The oil is stirred for 50 minutes under the condition of 40r / min, and the oil slurry scale inhibitor of the catalytic cracking unit is obtained.

Embodiment 2

[0030] This embodiment provides a kind of preparation method of the oil slurry antiscalant of catalytic cracking unit:

[0031] Stir 10kg of benzoic acid, 10kg of methyl hydroquinone, 30kg of polyacrylamide, 10kg of trans oleylamine ethyl imidazoline, 25kg of methanol and 15kg of 200# solvent oil under the condition of 50r / min for 60min to obtain catalytic cracking Slurry antiscalant for equipment.

Embodiment 3

[0033] This embodiment provides a kind of preparation method of the oil slurry antiscalant of catalytic cracking unit:

[0034] The composition of 7.5kg N-nitroso diphenylamine, 7.5kg 2-tert-butyl hydroquinone and methyl hydroquinone, the composition of 27.5kg sodium lauryl sulfate and polyacrylamide, 7.5kg cis The composition of oleic acid amine ethyl imidazoline, 20kg of xylene and methanol, and 30kg of 200# solvent oil were stirred for 55min under the condition of 45r / min to obtain the oil slurry scale inhibitor of the catalytic cracking unit.

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Abstract

The invention relates to an oil slurry scale inhibitor of a catalytic cracking unit and a preparation method thereof. The scale inhibitor is prepared from the following raw materials in percentage byweight: 5 to 10 percent of a scorch retarder, 5 to 10 percent of a polymerization inhibitor, 25 to 30 percent of a dispersing agent, 15 to 25 percent of a cleaning agent, 5 to 10 percent of a corrosion inhibitor and the balance of solvent. According to the preparation method, all the raw materials are mixed and stirred. The scale inhibitor can effectively inhibit scale deposition of an oil slurryand residual oil system; and the scale can be effectively removed in a short time to ensure the normal circulation of the slurry oil system, thereby stabilize the normal operation of the fractionationsystem and the vacuum residue system, lower the outlet pressure of the slurry oil pump, save energy, reduce consumption, ensure the product quality, and ensure the high-efficiency, high-quality and stable operation of the device. The preparation method is simple and easy to control, and large-scale production is facilitated.

Description

technical field [0001] The invention belongs to the field of scale inhibitors, and in particular relates to an oil slurry scale inhibitor for a catalytic cracking unit and a preparation method thereof. Background technique [0002] The catalytic cracking unit is the core unit of secondary processing. With the increasing weight of catalytic cracking raw materials, the scaling and coking problems of equipment not only run for a fixed period, but also directly affect the safe operation of equipment. Refining workers have proposed a series of solutions to the fouling problem from different perspectives such as equipment, process, and operation, such as lowering the temperature at the bottom of the fractionating tower, reducing the residence time, increasing the flow rate of the oil slurry, and installing an oil slurry filter. Certain effects, but there are certain limitations. [0003] The fouling problem of the fractionation tower bottom oil slurry system of the catalytic cra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G75/04C10G75/02
CPCC10G75/02C10G75/04
Inventor 庄锁良
Owner 北京乐文科技发展有限公司
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