Organic compound, display panel and display device
A technology of organic compounds and display panels, applied in the fields of organic compounds, display panels and display devices, can solve problems such as energy loss, achieve high polarizability and refractive index, improve luminous efficiency, and improve light extraction efficiency
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Embodiment 1
[0100] The synthetic route of compound CP001:
[0101]
[0102] In a 250 mL round bottom flask, 2-bromo-4,6-diiodo-pyrimidine (10 mmol), 6-boronic acid-isoquinoline (12 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol) aqueous solution (10mL), and the reaction was refluxed under nitrogen atmosphere for 12h. The resulting mixture was cooled to room temperature, added to water, and filtered through a pad of celite. The filtrate was extracted with dichloromethane, washed with water, and dried over anhydrous magnesium sulfate. After filtration and evaporation, the crude product was purified by silica gel column chromatography The intermediate product CP001-1 was obtained.
[0103] In a 250 mL round bottom flask, the intermediate product CP001-1 (10 mmol), 2-boronic acid-anthracene (22 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol...
Embodiment 2
[0106] The synthetic route of compound CP003:
[0107]
[0108] In a 250 mL round bottom flask, 4-bromo-2,6-diiodo-pyridine (10 mmol), 6-boronic acid-isoquinoline (12 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol) aqueous solution (10mL), and the reaction was refluxed under nitrogen atmosphere for 12h. The resulting mixture was cooled to room temperature, added to water, and filtered through a pad of celite. The filtrate was extracted with dichloromethane, washed with water, and dried over anhydrous magnesium sulfate. After filtration and evaporation, the crude product was purified by silica gel column chromatography The intermediate product CP003-1 was obtained.
[0109] In a 250 mL round bottom flask, the intermediate product CP003-1 (10 mmol), 2-boronic acid-anthracene (22 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol) ...
Embodiment 3
[0112] Synthetic route of compound CP011
[0113]
[0114] In a 250 mL round bottom flask, 2-bromo-4,6-diiodo-pyrimidine (10 mmol), 5-boronic acid-isoquinoline (12 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol) aqueous solution (10mL), and the reaction was refluxed under nitrogen atmosphere for 12h. The resulting mixture was cooled to room temperature, added to water, and filtered through a pad of celite. The filtrate was extracted with dichloromethane, washed with water, and dried over anhydrous magnesium sulfate. After filtration and evaporation, the crude product was purified by silica gel column chromatography The intermediate product CP011-1 was obtained.
[0115] In a 250 mL round bottom flask, the intermediate product CP011-1 (10 mmol), 2-boronic acid-anthracene (22 mmol) and Pd(PPh 3 ) 4 (0.3mmol) was added to a mixture of toluene (30mL) / ethanol (20mL) and potassium carbonate (12mmol) aqu...
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