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Organic compound, preparation method and application thereof

A technology of organic compounds and compounds, applied in organic chemistry, chemical instruments and methods, semiconductor/solid-state device manufacturing, etc., can solve problems such as unsatisfactory light-emitting area, low glass transition temperature, and low efficiency

Active Publication Date: 2020-03-24
NINGBO LUMILAN NEW MATERIAL CO LTD
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Problems solved by technology

[0003] CBP, the structural formula is It is a widely used host material with good hole transport properties. However, when CBP is used as a host material, due to the low glass transition temperature of CBP, it is easy to recrystallize, resulting in a decrease in the performance and luminous efficiency of OLED devices.
On the other hand, CBP is a hole-type host material, the transport of electrons and holes is unbalanced, the recombination efficiency of excitons is low, the light-emitting area is not ideal, and the roll-off phenomenon of the device is serious during operation, which leads to the Low efficiency of energy transfer from host material to guest material reduces device efficiency

Method used

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  • Organic compound, preparation method and application thereof
  • Organic compound, preparation method and application thereof
  • Organic compound, preparation method and application thereof

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preparation example Construction

[0147] Concrete synthesis method comprises the following steps:

[0148] Synthesis of C'-1: In a 250 ml three-necked flask, A'-1 (28.6 grams, 0.1mol), B'-1 (12.2 grams, 0.1mol), potassium carbonate (16.6 grams, 0.12 mol), toluene (100 ml), water (25 ml), tetrakis(triphenylphosphine)palladium (5.8 g, 0.005 mol), stirred at 100° C. for 10 hours, cooled to room temperature after reaction. The reaction system was added with water, extracted with dichloromethane, and the obtained extract was sequentially added to magnesium sulfate to dry, filtered and spin-dried; the crude product was purified by chromatography (the volume ratio of ethyl acetate / hexane was 1:10) to obtain C'-1 (22 g, 78% yield).

[0149] Synthesis of D'-1: In a 100 ml three-necked flask, add C'-1 (14.1 g, 0.05 mol), cuprous iodide (0.5 g, 2.5 mmol), cesium carbonate (19.6 g, 0.06 mol), 1,4-dioxane (60 milliliters), PAC (5mmol), nitrogen protection, heating and reflux for 20 hours, after the completion of the reac...

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Abstract

The invention provides an organic compound, a preparation method and application thereof. The organic compound has a structure shown as formula I in the specification, the organic compound has high thermal decomposition temperature, high triplet state energy level and small energy level difference between HOMO and LUMO, the HOMO and LUMO energy levels of a specific structure compound match a holetransport layer and an electron transport layer, at the same time, a specific three-dimensional configuration does not cause stacking of material molecules, reduces annihilation caused by the existence of high-energy excitons, improves the energy transfer efficiency, improves the luminous efficiency, and lowers the driving voltage, the organic compound has high luminous stability, effectively reduces color cast, has high thermal decomposition temperature and high thermal stability, and improves the luminous efficiency and luminous performance of devices.

Description

technical field [0001] The invention belongs to the technical field of organic photoelectric materials, and relates to an organic compound and its preparation method and application. Background technique [0002] Compared with traditional technologies, OLED devices have many advantages such as low driving voltage, high luminous efficiency, high contrast, high color saturation, wide viewing angle and fast response time. Today's OLED devices include multiple layers of hole injection layer, hole transport layer, light emitting layer, hole blocking layer, electron transport layer and electron injection layer, and are matched with suitable electrodes. These layers are composed of the following materials: Hole injection materials, hole transport materials, luminescent materials, hole blocking materials, electron transport materials and electron injection materials. Among them, the OLED light-emitting layer made by doping has advantages in the luminous efficiency of the device, so ...

Claims

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Application Information

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IPC IPC(8): C07D401/14C07D403/04C07D403/10C07D403/14C07D405/10C07D405/14C07D409/14C07D413/10C07D413/14C07D417/10C07D471/04C07D491/048C07D495/04C09K11/06H01L51/50H01L51/54
CPCC07D403/04C07D401/14C07D471/04C07D495/04C07D491/048C07D405/14C07D409/14C07D403/14C07D413/10C07D413/14C07D403/10C07D417/10C07D405/10C09K11/06C09K2211/1029C09K2211/1044C09K2211/1051C09K2211/1048C09K2211/1059C09K2211/1092C09K2211/1088H10K85/656H10K85/6565H10K85/636H10K85/631H10K85/654H10K85/6576H10K85/6572
Inventor 李祥智蔡烨丁欢达魏定纬陈志宽
Owner NINGBO LUMILAN NEW MATERIAL CO LTD
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