Method for adding nano particles into steel, refining structure and strengthening and toughening steel
A nano-particle strengthening and toughening technology, which is applied in the field of adding nanoparticles to steel and its refined structure and strengthening and toughening steel, can solve the problem of large specific surface area of nanoparticles, loss of grain refinement, and easy agglomeration and growth and other problems, to achieve the effect of simple process, improved wettability and low cost
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Embodiment 1
[0030] A method for adding nanoparticles to steel and refining its structure and strengthening and toughening steel, comprising the following steps:
[0031] (1) Pre-dispersion of nanoparticles
[0032] Weigh MgO nanopowder and metal aluminum nanopowder according to the mass ratio of 1:6, mix the two, and pre-disperse them in a planetary ball mill under vacuum and liquid nitrogen cooling conditions. The rotation speed is controlled at 1200rad / min, and the mixing time 12h, the mixed nanopowder was obtained.
[0033] (2) Preparation of aluminum-based intermediates
[0034] After melting metal aluminum in an intermediate frequency induction furnace, place the crucible with aluminum liquid in a spiral electromagnetic stirrer, insert the ultrasonic probe into the aluminum liquid, and turn on the spiral electromagnetic stirrer and ultrasonic processor at the same time. The temperature of the aluminum liquid is 850°C. Add and disperse and mix nano-powder into the aluminum liquid, t...
Embodiment 2
[0039] A method for adding nanoparticles and its refined structure and strengthening and toughening steel to steel, the basic experimental steps of this embodiment are the same as those of Example 1, the difference is that the volume of MgO nano powder in the aluminum-based intermediate is obtained The fraction is 16.6%, and the mass fraction of MgO nanopowder in the continuous casting slab is 0.0068%.
Embodiment 3
[0041] A method for adding nanoparticles and its refined structure and strengthening and toughening steel to steel, the basic experimental steps of this embodiment are the same as those of Example 1, the difference is that the volume of MgO nano powder in the aluminum-based intermediate is obtained The fraction is 18.4%, and the mass fraction of MgO nanopowder in the continuous casting slab is 0.0082%.
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