Acidic biochar fertilizer suitable for saline-alkali soil and preparation method thereof
A biochar, saline-alkali land technology, applied in the application, fertilization device, fertilizer mixture and other directions, can solve the problems that the saline-alkali soil cannot provide enough organic matter, cannot significantly reduce soil pH, and has limited ability to reduce soil pH, etc., and achieves far-reaching social significance. and economic value, the preparation method is simple and controllable, and the effect of improving food and agricultural security
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Embodiment 1
[0021] (1) Preparation of biochar: Clean up the collected yak dung, dry it, crush it through a 40-mesh sieve, take 10 g of the sieved yak dung and mix it with 50 mL of deionized water and place it in a hydrothermal reaction kettle. Mpa nitrogen repeatedly purged the reactor for 3 times, carried out hydrothermal reaction at 150°C, stirred at a speed of 100r / min, stayed for 0.5h when reaching the final temperature, cooled to room temperature, and washed the hydrothermal solution with absolute ethanol until Colorless, then washed with distilled water until neutral, then suction filtered, and the solid product was dried to obtain biochar;
[0022] (2) Preparation of acidic biochar fertilizer: Take 2g of biochar obtained in step (1) and mix with 20mL of 0.05mol / L nitric acid, shake in a shaker at 25°C and 120r / min for 6h, and rinse with deionized water after the end Wash to adjust the pH value and filter with suction. After drying at 100°C, pass through a 60-mesh sieve to obtain ac...
Embodiment 2
[0025] (1) Preparation of biochar: Clean up the collected yak dung, dry it, crush it through a 50-mesh sieve, take 10 g of the sieved yak dung and mix it with 60 mL of deionized water and place it in a hydrothermal reaction kettle. Mpa nitrogen repeatedly purged the reactor for 3 times, carried out hydrothermal reaction at 180°C, stirred at a speed of 110r / min, stayed for 1h when the final temperature was reached, cooled to room temperature, and washed the hydrothermal solution with absolute ethanol until it was completely dry. color, and then washed with distilled water until neutral, then suction filtered, and the solid product was dried to obtain biochar;
[0026] (2) Preparation of acidic biochar fertilizer: Take 2g of biochar obtained in step (1) and mix with 30mL of 0.06mol / L nitric acid, shake in a shaker at 28°C and 140r / min for 12h, and rinse with deionized water after the end Wash to adjust the pH value and filter with suction. After drying at 105°C, pass through a 7...
Embodiment 3
[0029] (1) Preparation of biochar: Clean up the collected yak dung, dry it, crush it through a 60-mesh sieve, take 10 g of the sieved yak dung and mix it with 70 mL of deionized water and place it in a hydrothermal reaction kettle. Mpa nitrogen repeatedly purged the reactor for 3 times, carried out hydrothermal reaction at 200°C, stirred at a speed of 120r / min, stayed for 1.5h when reaching the final temperature, cooled to room temperature, and washed the hydrothermal solution with absolute ethanol to Colorless, then washed with distilled water until neutral, then suction filtered, and the solid product was dried to obtain biochar;
[0030] (2) Preparation of acidic biochar fertilizer: Take 2g of biochar obtained in step (1) and mix with 40mL of 0.1mol / L nitric acid, shake in a shaker at 30°C and 150r / min for 24h, and rinse with deionized water after the end Wash to adjust the pH value and filter with suction. After drying at 110°C, pass through an 80-mesh sieve to obtain acid...
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