Method for assembling large aspect ratio probe
A technology with a large aspect ratio and an assembly method, which is applied in scanning probe technology, scanning probe microscopy, measuring devices, etc., can solve problems such as scratches, and achieve cost saving, excellent mechanical properties, and non-wearing effects
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Embodiment 1
[0038] 1) Hydrophilic treatment of needle tip
[0039] First, rinse the needle tip with ethanol for 8 minutes; configure the hydrophilic solution according to the volume ratio of ammonia water: hydrogen peroxide: deionized water = 1:1:5, with a total volume of 250 mL. Clamp the needle tip on the fixture and put it into a beaker, pour 125mL of the hydrophilic solution into the beaker and cover it, put the beaker into an oil-bath insulation pot to keep the heating temperature at 80°C, and take it out after constant heating for 1.5h.
[0040] 2) Configuration of carbon nanotube mixed solution
[0041] Use a measuring cylinder to measure 3-aminopropyltriethoxysilane and isopropanol solution respectively, and configure 250mL mixed solution A according to the ratio of 1:9; disperse the multi-walled carbon nanotube powder evenly in the isopropanol solvent , the dispersion concentration is 0.00025mg / mL, then add the above mixed solution A to fully ultrasonically disperse, and the ult...
Embodiment 2
[0046] 1) Hydrophilic treatment of needle tip
[0047] First, rinse the needle tip with ethanol for 5 minutes; configure the hydrophilic solution according to the volume ratio of ammonia water: hydrogen peroxide: deionized water = 1:1:5, with a total volume of 50 mL. Clamp the needle tip on the fixture and put it into a beaker, pour 25mL of the hydrophilic solution into the beaker and cover it, put the beaker into an oil-bath insulation pot to keep the heating temperature at 75°C, and take it out after constant heating for 0.5h.
[0048] 2) Configuration of silicon oxide nanowire mixed solution
[0049] Use a graduated cylinder to measure 3-aminopropyltriethoxysilane and isopropanol solution respectively, and configure 25mL of mixed solution A according to the ratio of 1:8; disperse the silicon oxide nanowire powder evenly in the isopropanol solvent, The dispersion concentration is 0.00004 mg / mL, and then the above mixed solution A is added to fully ultrasonically disperse, a...
Embodiment 3
[0053] 1) Hydrophilic treatment of needle tip
[0054] First, rinse the needle tip with ethanol for 10 minutes; configure the hydrophilic solution according to the volume ratio of ammonia water: hydrogen peroxide: deionized water = 1:1:5, with a total volume of 500 mL. Clamp the needle tip on the fixture and put it into a beaker, pour 250mL of the hydrophilic solution into the beaker and cover it, put the beaker into an oil-bath insulation pot to keep the heating temperature at 85°C, and take it out after constant heating for 2 hours.
[0055] 2) Configuration of ZnO nanorod mixed solution
[0056] Use a measuring cylinder to measure 3-aminopropyltriethoxysilane and isopropanol solution respectively, and configure 500mL of mixed solution A according to the ratio of 1:10; uniformly disperse the zinc oxide nanorod powder in the isopropanol solvent, The dispersion concentration is 0.0005mg / mL, and then the above mixed solution A is added to fully ultrasonically disperse, and the...
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