A kind of high-strength and low-shrinkage air-entrained concrete and its preparation method
An air-entrained concrete and low-shrinkage technology, which is applied in the field of air-entrained concrete, can solve the problems of low production efficiency, high water absorption, and large shrinkage, and achieve the effects of improving production efficiency, shortening time, reducing water absorption and drying shrinkage
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Embodiment 1
[0029] A B04 grade lightweight sand aerated concrete is prepared by the following steps:
[0030] S1: Use a 500ml measuring cylinder to measure 150ml of industrial ethanol and pour it into a 1000ml four-neck flask, slowly add 50ml of stearic acid dropwise into the flask, and stir until the stearic acid is completely dissolved in the industrial ethanol, then Add 300ml of 2.5mol / L calcium chloride solution to the mixed solution, stir evenly, add 300ml of 2.5mol / L sodium carbonate solution to the aforementioned mixed solution, and carry out the polymerization reaction for 2~3h to obtain nano-carbonic acid salt crystals, then add 20ml of 1mol / L TiC solution into the four-necked flask, place it at 60-70°C for 6-8h, after the reaction is complete, slowly cool down to room temperature for 1-2h, and stir at 3000-5000rpm for 1 ~2min, the modified nano-calcium carbonate gel solution with a solid content of 47.5% and a nanoparticle size of 65.4nm is obtained for subsequent use;
[0031]...
Embodiment 2
[0037] A B05 grade lightweight sand aerated concrete is prepared by the following steps:
[0038] S1: Use a 500ml graduated cylinder to measure 150ml of trimethylolpropane and pour it into a 1000ml four-neck flask, slowly add 80ml of palmitic acid dropwise into the flask, and stir until the stearic acid is completely dissolved in industrial ethanol , then add 350ml of 2.5mol / L magnesium chloride solution to the mixed solution, stir evenly, add 320ml of 2.5mol / L sodium carbonate solution to the aforementioned mixed solution, and carry out the polymerization reaction for 2~3h to obtain nano-carbonic acid salt crystals, then add 25ml of 1mol / L TaC solution into the four-necked flask, place it at 60-70°C for 6-8h, and after the reaction is complete, cool slowly for 1-2h to room temperature, and stir at 3000-5000rpm for 1~ 2min, promptly obtain the modified nano-magnesium carbonate gel solution that solid content is 48.2% and nanoparticle particle diameter is 75nm, for subsequent u...
Embodiment 3
[0045] A B06 grade lightweight sand aerated concrete is prepared by the following steps:
[0046] S1: Measure 150ml of ethylene glycol with a 500ml measuring cylinder and pour it into a 1000ml four-neck flask, slowly add 60ml of linolenic acid dropwise into the flask, and stir while adding until the stearic acid is completely dissolved in industrial ethanol, then Add 320ml of 2.5mol / L lithium chloride solution to the mixed solution, stir evenly, add 350ml of 2.5mol / L sodium carbonate solution to the aforementioned mixed solution, and carry out the polymerization reaction for 2~3h to obtain nano-carbonic acid Salt crystals, then add 30ml of 1mol / L Cr in the four-necked flask 3 C 2 Solution, placed at 60-70°C for 6-8 hours, after the reaction was complete, slowly cooled for 1-2 hours to room temperature, and stirred at 3000-5000rpm for 1-2 minutes to obtain a solid content of 46.8% and a particle size of 54.7nm The modified nano lithium carbonate gel solution;
[0047] S2: Ac...
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