Mask material for surface surgery anesthesia and preparation method thereof
A facial mask and surgery technology, which is applied in the field of facial mask materials for surface surgical anesthesia and its preparation, can solve the problems of slow onset, poor compliance, and unfavorable recovery of traditional Chinese medicine, and achieve fast onset, strong effect, and good effect
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Embodiment 1
[0028] A preparation method for surface surgical anesthesia mask material, comprising the steps of:
[0029] Ⅰ Preparation of cis-3-hexenol lactate / 2-ethylhexyl ether diethylene glycol acrylate / polyethylene glycol monoallyl ether / 3-chloro-2-hydroxypropyl acrylate copolymer: cis-3-hexenol lactate 1kg, 2-ethylhexyl ether diethylene glycol acrylate 1kg, polyethylene glycol monoallyl ether 1kg, 3-chloro-2-hydroxypropyl acrylate 0.3kg , mixed with 0.02kg of benzoin, ultrasonicated at 40°C for 10 minutes, then poured into a mold, then placed the mold in a nitrogen atmosphere, and irradiated with ultraviolet light with a wavelength of 200nm for 30 minutes to obtain cis-3-hexenol Lactate / 2-Ethylhexyl Ether Diethylene Glycol Acrylate / Polyethylene Glycol Monoallyl Ether / 3-Chloro-2-Hydroxypropyl Acrylate Copolymer;
[0030] II Acepromazine graft copolymer: Add 1kg of the copolymer prepared in step I and 0.1kg of acepromazine into 3kg of dimethyl sulfoxide, stir and react at 40°C for 3 h...
Embodiment 2
[0037] A preparation method for surface surgical anesthesia mask material, comprising the steps of:
[0038] Ⅰ Preparation of cis-3-hexenol lactate / 2-ethylhexyl ether diethylene glycol acrylate / polyethylene glycol monoallyl ether / 3-chloro-2-hydroxypropyl acrylate copolymer: cis-3-hexenol lactate 1kg, 2-ethylhexyl ether diethylene glycol acrylate 1kg, polyethylene glycol monoallyl ether 1kg, 3-chloro-2-hydroxypropyl acrylate 0.35kg , mixed with 0.025kg of benzoin ethyl ether, ultrasonicated at 45°C for 12 minutes, then poured into a mold, then placed the mold in a helium atmosphere, and irradiated with ultraviolet light with a wavelength of 210nm for 32 minutes to obtain cis-3-hexyl Enol lactate / 2-ethylhexyl ether diethylene glycol acrylate / polyethylene glycol monoallyl ether / 3-chloro-2-hydroxypropyl acrylate copolymer;
[0039] II Acepromazine graft copolymer: Add 1kg of the copolymer prepared in step I and 0.1kg of acepromazine into 3.5kg of N,N-dimethylformamide, stir and r...
Embodiment 3
[0046] A preparation method for surface surgical anesthesia mask material, comprising the steps of:
[0047] Ⅰ Preparation of cis-3-hexenol lactate / 2-ethylhexyl ether diethylene glycol acrylate / polyethylene glycol monoallyl ether / 3-chloro-2-hydroxypropyl acrylate copolymer: cis-3-hexenol lactate 1kg, 2-ethylhexyl ether diethylene glycol acrylate 1kg, polyethylene glycol monoallyl ether 1kg, 3-chloro-2-hydroxypropyl acrylate 0.4kg , mixed with 0.03kg of benzoin dimethyl ether, ultrasonicated at 50°C for 15 minutes, then poured into a mold, then placed the mold in a helium atmosphere, and irradiated with ultraviolet light with a wavelength of 210nm for 33 minutes to obtain cis-3 - Hexenyl lactate / 2-ethylhexyl ether diethylene glycol acrylate / polyethylene glycol monoallyl ether / 3-chloro-2-hydroxypropyl acrylate copolymer;
[0048] II Acepromazine graft copolymer: add 1kg of the copolymer prepared in step I and 0.1kg of acepromazine into 4kg of N-methylpyrrolidone, stir and react...
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