Composite soft magnetic metal powder, preparation method and integrally-formed inductor
A metal powder, composite soft magnetic technology, applied in metal processing equipment, inductance/transformer/magnet manufacturing, circuits, etc., can solve the problems of sacrificing integrated inductance magnetic
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[0028] The invention provides a method for preparing composite soft magnetic metal powder, comprising the following steps:
[0029] Step S1, passivation treatment: the soft magnetic metal powder is placed in a phosphorus-containing solution for phosphating reaction, so that a phosphating film is formed on the surface of the soft magnetic metal powder, then filtered, dried, and set aside;
[0030] Step S2, preparing a coating agent: adding rare earth oxides to the adhesive, mixing evenly and then setting aside;
[0031] Step S3, adding the soft magnetic metal powder obtained in step S1 to the coating agent obtained in step S2, and mixing evenly;
[0032] Step S4, granulating and drying the mixture obtained in step S3;
[0033] Step S5, adding a lubricant to the particles obtained in step S4, and mixing uniformly to obtain the composite soft magnetic metal powder.
[0034] Wherein, the soft magnetic metal powder is carbonyl iron powder or iron-silicon-chromium alloy powder; th...
Embodiment 1
[0038] Step S1. Soak the carbonyl iron powder in a zinc-based phosphating solution with a mass fraction of 0.5% until a phosphating film is formed on the surface of the carbonyl iron powder, filter off the liquid, and dry the solid in a draft oven. The temperature is 150°C, and the baking time is 120 minutes, then take it out and let it dry for later use.
[0039] Step S2, adding samarium oxide powder and absolute ethanol to the phenolic resin, followed by stirring in a water bath at 40°C to obtain a uniform mixed coating agent, which is ready for use.
[0040] In this step, the amount of samarium oxide is 2% of the mass of carbonyl iron powder, the volume ratio of phenolic resin to absolute ethanol is 1:5, and the amount of phenolic resin is equivalent to that of conventional methods.
[0041] Step S3, adding the solid obtained in step S1 to the coating agent obtained in step S2, stirring evenly, and then granulating to obtain wet powder.
[0042] Step S4, put the wet powder...
Embodiment 2
[0047] Step S1, soak the carbonyl iron powder in a zinc-based phosphating solution with a mass fraction of 1.5% to form a phosphating film on the surface of the carbonyl iron powder, filter off the liquid, dry the solid in a draft oven, and bake The temperature is 150°C, and the baking time is 120 minutes, then take it out and let it dry for later use.
[0048] Step S2, adding cerium oxide powder and acetone to the phenolic resin, followed by stirring in a water bath at 45°C to obtain a uniform mixed coating agent, which is ready for use.
[0049] In this step, the consumption of described cerium oxide is 5% of carbonyl iron powder quality, diluent is dehydrated alcohol, and the consumption volume ratio of phenolic resin and dehydrated alcohol is 1: 3, the consumption of phenolic resin and conventional method consumption quite.
[0050] Step S3, adding the solid obtained in step S1 to the coating agent obtained in step S2, stirring evenly, and then granulating to obtain wet p...
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