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Metal/ceramic composite material and preparation method based on titanium silicon carbide ceramics and copper

A ceramic composite material, titanium silicon carbide technology, applied in the field of composite materials, can solve the problems of low thermal shock resistance of composite materials, low bonding strength of ceramic phase grains, etc., and achieve stable material properties, simple molding equipment, and stable and reliable process. Effect

Active Publication Date: 2022-01-11
张永利
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] As early as the late 1990s, Zhu Chuncheng of Harbin Institute of Technology and others reported the preparation of TiB2-TiC / Cu-Ni by using metal titanium, boron carbide, metal copper powder and nickel powder as raw materials through pressurized self-propagating high-temperature synthesis technology. Ablation-resistant materials, but due to the low bonding strength of the ceramic phase grains in the prepared composite materials, the thermal shock resistance of the composite materials is low, and there are no reports of subsequent applications

Method used

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  • Metal/ceramic composite material and preparation method based on titanium silicon carbide ceramics and copper
  • Metal/ceramic composite material and preparation method based on titanium silicon carbide ceramics and copper
  • Metal/ceramic composite material and preparation method based on titanium silicon carbide ceramics and copper

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Effect test

Embodiment 1

[0039] refer to figure 1 , a method for preparing a metal / ceramic composite material based on titanium silicon carbide ceramics and copper, carried out according to the following steps:

[0040](1) Preparation of ceramic green body: put 200-400M titanium silicon carbide powder and 80M sieved phenolic resin powder (mass ratio is 17:3) in a planetary ball mill at a speed of 300r / min, mix for 5h, and mix the powder Put it in a stainless steel mold coated with boron nitride release agent, carry out warm pressing molding on a flat vulcanizing machine, set the temperature of the upper and lower platens of the flat vulcanizing machine to 180°C, and the pressure to 10MPa, hold the pressure for 30min, and get a ceramic green body after demoulding .

[0041] (2) Preparation of porous ceramics: ceramic green body in N 2 Pyrolysis under atmosphere protection, carbonization of phenolic resin, atmospheric pressure (1atm), nitrogen flow rate 0.5L / min, heating to 650°C at a heating rate of ...

Embodiment 2

[0046] refer to figure 1 , a method for preparing a metal / ceramic composite material based on titanium silicon carbide ceramics and copper, carried out according to the following steps:

[0047] (1) Preparation of ceramic green body: put 200-400M titanium silicon carbide powder and 80M sieved phenolic resin powder (mass ratio is 17:3) in a planetary ball mill at a speed of 300r / min, mix for 5h, and mix the powder Put it in a stainless steel mold coated with boron nitride release agent, carry out warm pressing molding on a flat vulcanizing machine, set the temperature of the upper and lower platens of the flat vulcanizing machine to 180°C, and the pressure to 10MPa, hold the pressure for 30min, and get a ceramic green body after demoulding .

[0048] (2) Preparation of porous ceramics: ceramic green body in N 2 Pyrolysis under atmosphere protection, carbonization of phenolic resin, atmospheric pressure (1atm), nitrogen flow rate 0.5L / min, heating to 650°C at a heating rate of...

Embodiment 3

[0052] refer to figure 1 , a method for preparing a metal / ceramic composite material based on titanium silicon carbide ceramics and copper, carried out according to the following steps:

[0053] (1) Preparation of ceramic green body: put 200-400M titanium silicon carbide powder and 80M sieved phenolic resin powder (mass ratio is 17:3) in a planetary ball mill at a speed of 300r / min, mix for 5h, and mix the powder Put it in a stainless steel mold coated with boron nitride release agent, carry out warm pressing molding on a flat vulcanizing machine, set the temperature of the upper and lower platens of the flat vulcanizing machine to 180°C, and the pressure to 10MPa, hold the pressure for 30min, and get a ceramic green body after demoulding .

[0054] (2) Preparation of porous ceramics: ceramic green body in N 2 Pyrolysis under atmosphere protection, carbonization of phenolic resin, atmospheric pressure (1atm), nitrogen flow rate 0.5L / min, heating to 650°C at a heating rate of...

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Abstract

The invention provides a layered ceramic titanium silicon carbide based on MAX phase (Ti 3 SiC 2 ) and metal copper composite material, comprising the following steps: (1) mixing: mixing titanium silicon carbide powder and resin powder in a ball mill and drying to obtain mixed powder. (2) Warm pressing molding: the mixed powder is placed in a mold, heated and pressed to form a green body. (3) Pyrolysis: The green body is pyrolyzed in a nitrogen environment to obtain a mixed skeleton of porous carbon and ceramics. (4) Reaction sintering to obtain porous ceramics. (5) Vacuum infiltration: Melt and impregnate porous ceramics with copper under vacuum to obtain metal / ceramic composite materials. The prepared composite material has a continuous three-dimensional network structure in which ceramics and metals interweave, exhibits good mechanical properties, and also has good electrical properties and wear resistance, and has a simple preparation method and has broad application prospects.

Description

technical field [0001] The invention relates to the technical field of composite materials, in particular to a metal / ceramic composite material based on titanium silicon carbide ceramics and copper, a preparation method and application thereof. Background technique [0002] Ceramic / metal composite materials have excellent mechanical properties, electrical and thermal conductivity and friction and wear properties, and can be used as electrical, thermal and wear-resistant materials in harsh environments. The currently reported ceramic / metal composite materials are mainly ceramic particle-reinforced metal matrix composite materials, and the preparation processes are mainly powder metallurgy, discharge plasma reaction sintering, etc. [0003] MAX phase is a ternary layered metallic ceramic material, the general formula is M n+1 AX n , where M is a transition metal element, generally Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta; A is a main group element in the periodic table 13-16, ge...

Claims

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Application Information

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IPC IPC(8): C04B35/56C04B35/622C04B38/06C04B41/88
CPCC04B35/5615C04B35/622C04B38/068C04B41/009C04B41/5127C04B41/88C04B2235/3826C04B2235/3843C04B2235/602C04B2235/656C04B2235/6562C04B2235/6565C04B2235/6567C04B2235/96C04B41/4523
Inventor 张永利
Owner 张永利
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