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Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate and preparation method thereof

An aluminum alloy sheet and aluminum alloy technology, applied in the field of light metal material preparation and processing, can solve the problems of low production efficiency, long time consumption, complex alloy production process, etc., and achieve the effects of improving production efficiency, avoiding long time consumption, and improving comprehensive mechanical properties

Active Publication Date: 2019-07-02
YANTAI NANSHAN UNIV
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0005] To sum up, the problems existing in the existing technology are: the composition of the aluminum alloy needs to be continuously optimized, the alloy composition of the medium-strength and high-toughness aluminum alloy needs to be further optimized, the development of Cu-free, low-Zn medium-strength and high-toughness 7-series aluminum alloy varieties, adding Trace rare earth and transition group elements, control the proportion of microalloying elements, and obtain high-performance medium-strength and high-toughness 7-series aluminum alloy sheets
The alloy production process is complex and the production efficiency is relatively low, especially the homogenization heat treatment, which takes a long time. Therefore, it is necessary to continue to discuss the preparation process, optimize the heat treatment system, improve production efficiency, and achieve energy conservation and environmental protection on the basis of optimizing alloy elements.

Method used

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  • Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate and preparation method thereof
  • Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate and preparation method thereof
  • Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate and preparation method thereof

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preparation example Construction

[0034] The preparation method of the Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate provided by the embodiment of the present invention includes the following steps: batching, melting and casting, stress relief annealing, machining, heating, extrusion, Quenching, stretching straightening, aging.

[0035] Melt pure aluminum and all intermediate alloys together, the melting temperature is 760℃~790℃, add covering agent during melting, the covering agent is prepared by sodium chloride and potassium chloride according to the ratio of 1:1, after complete melting, refining and degassing, wait for When the temperature drops below 730°C, add pure zinc and pure magnesium. The pure magnesium is calculated according to the burning loss of 3-5%, and cast into an aluminum alloy cylindrical ingot of 300mm-500mm.

[0036] Aluminum alloy cylindrical ingots need to be annealed for stress relief in the range of 220-300 °C.

[0037] Homogenization annealing is not r...

Embodiment example 2

[0046] According to the ingredients and weight percentages of 3.0% Zn, 1.5% Mg, 0.4% Mn, 0.3% Cr, 0.2% Zr, 0.2% Er, 0.3Si and the rest are Al, Al-Mn, Al-Zr, Al-Er and Al-Cr master alloys, pure magnesium according to the proportion of burning loss of about 5%, pure aluminum (99.85%) and master alloys are melted at a temperature of 780°C at the same time, and covering agents are added during melting. Prepare sodium chloride and potassium chloride at a ratio of 1:1. After the alloy is completely melted, refining and degassing, slag removal, static cooling to 720°C, adding pure zinc (99.9%) and pure magnesium (99.9%) in turn, after the pure magnesium is completely melted, stirring, slag removal, at 710°C It is poured into an aluminum alloy cylindrical ingot with a diameter of 500mm at a certain temperature. The aluminum alloy cylindrical ingot according to After stress relieving annealing, after the saw head cuts the outer circle, it is slowly heated to 440°C, kept for 3 hours,...

Embodiment example 3

[0049] According to the composition and weight percentage of 2.8% Zn, 1.7% Mg, 0.3% Mn, 0.15% Cr, 0.2% Zr, 0.2% Er, 0.2Si, the rest is Al, and Al-Mn, Al-Zr, Al-Er and Al-Cr master alloys, pure magnesium according to the proportion of burning loss of about 5%, pure aluminum (99.85%) and master alloys are melted at a temperature of 780°C at the same time, and covering agents are added during melting. Prepare sodium chloride and potassium chloride at a ratio of 1:1. After the alloy is completely melted, refining and degassing, slag removal, static cooling to 720°C, adding pure zinc (99.9%) and pure magnesium (99.9%) in turn, after the pure magnesium is completely melted, stirring, slag removal, at 710°C It is poured into an aluminum alloy cylindrical ingot with a diameter of 300mm at a certain temperature. The aluminum alloy cylindrical ingot according to After stress relieving annealing, after the saw head cuts the outer circle, it is slowly heated to 440°C, kept for 3 hours,...

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Abstract

The invention discloses a preparation method of an Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate. The Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate is prepared from the alloy components: 3.0-4.0% of Zn, 1-2% of Mg, 0.2-0.4% of Mn, 0.1-0.3% of Cr, 0.1-0.3% of Zr, 0.1-0.3% of Er, 0.1-0.5% of Si, less than 0.01% of Cu and the balance of Aland other impurities, and the content of single impurity is not more than 0.1%. The preparation process includes the steps that an alloy prepared according to the composition design is smelted, casted and poured into an ingot with a diameter of 300 mm to 500 mm, the temperature is directly raised to 460 DEG C without homogenization heat treatment after stress relief annealing of the ingot is completed at 220 DEG C to 300 DEG C, after temperature is kept for 3 to 6 hours, hot extruding is carried out, and an aluminum alloy plate with a thickness of 6 to 10 mm is prepared under the condition that the extrusion ratio exceeds 16, wherein the extruded aluminum alloy plate has the tensile strength of more than 350 Mp, the yield strength of more than 300 Mp, the elongation of more than 15% and the ISSRT of less than 0.03 at normal temperature after solid solution aging treatment.

Description

technical field [0001] The invention belongs to the preparation of aluminum alloy plates and belongs to the technical field of preparation and processing of light metal materials, in particular to an Al-Zn-Mg-Cr-Mn-Zr-Er medium-strength and high-toughness aluminum alloy plate and a preparation method thereof. Background technique [0002] At present, the closest existing technology: 7-series aluminum alloys are mainly composed of Zn and alloying elements. According to the performance requirements of the alloy, it is also necessary to add an appropriate amount of Cu and Mg. Therefore, the so-called 7-series aluminum alloys are mainly Al - Zn-Mg-Cu alloy. At present, due to the advantages of low density, high strength and easy processing and forming, the 7-series aluminum alloy has been widely used in the fields of transportation and aerospace. [0003] With the world's high standards for energy and the environment, in order to achieve energy conservation and environmental pr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C21/10C22C1/03C22F1/053
CPCC22C1/026C22C1/03C22C21/10C22F1/002C22F1/053
Inventor 房洪杰初晋华史春丽李民孔德斌朱鹏程张涵源张彦芝程雪婷
Owner YANTAI NANSHAN UNIV
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