A method for preparing strontium-rich activated carbon by hydrothermal method
A technology of activated carbon and strontium-enriched technology, which is applied in the field of deep processing and preparation of activated carbon, can solve the problems of weak combination of active components and carriers, blockage of active component microcrystals, and reduced pore volume, so as to achieve the goal of increasing added value and reducing production costs Effect
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preparation example Construction
[0021] 1. Preparation of strontium-rich activated carbon by impregnation-hydrothermal method, including the following steps:
[0022] (a) Preprocessing process:
[0023] Place the proportioned activated carbon in a hydrochloric acid solution with a concentration of (4-10) wt% and heat while stirring, heat and boil the charcoal for 30-60 minutes, let it stand for 0.5 hours, then filter it with suction, and then wash the proportioned activated carbon repeatedly with pure water , Wash off the residual acid on the surface, boil it with pure water for 0.5-1 hour, rinse until the pH value is 6.5-8.5, and finally dry it at 105-120°C for use.
[0024] (b) Dip loading process:
[0025] Take an appropriate amount of activated carbon after pretreatment, place it in an excess sodium silicate solution with a concentration of 0.1-0.3 mol / L, immerse and stir for 10-20 minutes, and then add a strontium salt solution with a concentration of 0.05-0.5 mol / L in the impregnation solution, Mix an...
example 1
[0033] Take by weight 50 g of proportioning activated carbon above 150 mesh, and the mass proportioning ratio is 3:2. Place in a 3L beaker, slowly add 70g of diluted edible hydrochloric acid with a concentration of 4wt% into it while stirring, after stirring for 10 minutes, start heating, stir while heating, until the activated carbon solution boils for 40 minutes, and then suction filter after cooling for 0.5 hours. Then use pure water to wash the activated carbon repeatedly to remove the residual acid on the surface; then boil it with pure water for 0.5 hours, filter and rinse until the pH value is 6.5-8.5, that is, complete the process of hydrochloric acid deashing, and finally in the Dry at 105-120°C for later use.
[0034] Weigh 4 g of proportioned activated carbon after hydrochloric acid impurity removal pretreatment, place it in 600 mL of sodium silicate solution with a concentration of 0.2 mol / L and stir for 10 minutes, and then add 150 mL of chlorine with a concentrat...
example 2
[0037] Take by weight 50 g of proportioning activated carbon above 150 mesh, and the mass proportioning ratio is 3:2. Place in a 3L beaker, slowly add 70g of diluted edible hydrochloric acid with a concentration of 4wt% into it while stirring, after stirring for 10 minutes, start heating, stir while heating, until the activated carbon solution boils for 40 minutes, and then suction filter after cooling for 0.5 hours. Then use pure water to wash the activated carbon repeatedly to remove the residual acid on the surface; then boil it with pure water for 0.5 hours, filter and rinse until the pH value is 6.5-8.5, that is, complete the process of hydrochloric acid deashing, and finally in the Dry at 105-120°C for later use.
[0038] Weigh 4 g of proportioned activated carbon after hydrochloric acid impurity removal pretreatment, place it in 600 mL of sodium silicate solution with a concentration of 0.2 mol / L and stir for 10 minutes, and then add 150 mL of chlorine with a concentrat...
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