Treatment method of phenolic wastewater
A treatment method and technology for phenolic wastewater, applied in water/sewage treatment, light water/sewage treatment, oxidized water/sewage treatment, etc., can solve the problems of affecting the degradation of phenolic substances, reducing catalytic activity, easy agglomeration, etc., to achieve enhanced Phenolic substances, improve catalytic activity, solve the effect of agglomeration
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Embodiment 1
[0021] A kind of treatment method of phenolic waste water proposed by the present invention, comprises the following steps: in phenolic waste water, add H 2 o 2 , Fe 3 o 4 / PANI composite material, followed by microwave treatment.
[0022] Among them, Fe 3 o 4 / PANI composite material is prepared according to the following process:
[0023] S1, the nano-Fe 3 o 4 Mix with ethanol aqueous solution, ultrasonically treat, then add sodium lauryl sulfate and aniline, mix well, add concentrated hydrochloric acid, stir to obtain material A;
[0024] S2. Add ammonium persulfate aqueous solution to material A, stir, filter, wash, dry, and grind to obtain Fe 3 o 4 / PANI Composite.
Embodiment 2
[0026] A kind of treatment method of phenol-containing wastewater proposed by the present invention comprises the following steps: adding 0.15 parts of concentration of 25wt% H to 40 parts of phenol-containing wastewater by weight 2 o 2 , 40 parts of Fe 3 o 4 / PANI composite material, and then carry out microwave treatment, wherein, microwave power is 70W, and microwave treatment time is 6min.
[0027] Among them, Fe 3 o 4 / PANI composite material is prepared according to the following process:
[0028] S1, by weight 0.02 parts of nano-Fe 3 o 4 Mix with 100 parts of ethanol aqueous solution with a volume concentration of 8%, ultrasonically treat for 20min, then add 0.01 part of sodium lauryl sulfate and 0.4 part of aniline, mix well, add 5 parts of concentrated hydrochloric acid with a concentration of 35wt%, and stir at room temperature 40min, get material A;
[0029] S2. Add 9 parts of ammonium persulfate aqueous solution with a concentration of 6wt% to material A, s...
Embodiment 3
[0031] A kind of treatment method of phenol-containing wastewater proposed by the present invention comprises the following steps: adding 0.3 parts of concentration of 35wt% H to 60 parts of phenol-containing wastewater by weight 2 o 2 , 60 parts of Fe 3 o 4 / PANI composite material, and then carry out microwave treatment, wherein, microwave power is 210W, and microwave treatment time is 4min.
[0032] Among them, Fe 3 o 4 / PANI composite material is prepared according to the following process:
[0033] S1, by weight 0.03 parts of nano-Fe 3 o 4 Mix with 120 parts of ethanol aqueous solution with a volume concentration of 12%, ultrasonically treat for 15min, then add 0.02 parts of sodium lauryl sulfate and 0.6 parts of aniline, mix well, add 7 parts of concentrated hydrochloric acid with a concentration of 40wt%, and stir at room temperature 30min, obtain material A;
[0034] S2. Add 11 parts of ammonium persulfate aqueous solution with a concentration of 8wt% to materia...
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