Liquid crystal alignment agent, liquid crystal alignment film, liquid crystal display element, and novel monomer
A liquid crystal and display technology, applied in the field of polymers, can solve problems such as dust generation, static electricity, and even rubbing of liquid crystal alignment films
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[0377] [Preparation of polymer composition]
[0378] The polymer composition used in the present invention is preferably prepared as a coating liquid in a manner suitable for forming a liquid crystal aligning film. That is, the polymer composition used in the present invention is preferably prepared in the form of a solution in which the above-mentioned component (A) and the above-mentioned solvent for improving film thickness uniformity and surface smoothness, compounds, A compound etc. for improving the adhesiveness of a liquid crystal aligning film and a board|substrate. Here, content of (A) component becomes like this. Preferably it is 1 mass % - 20 mass %, More preferably, it is 3 mass % - 15 mass %, Especially preferably, it is 3 mass % - 10 mass %.
[0379] In the polymer composition of this embodiment, other polymers other than the component (A) may be mixed within a range not impairing liquid crystal expressiveness and photosensitivity. In this case, content of othe...
Embodiment
[0439] Examples are given below to describe the present invention in more detail, but the present invention is not limited thereto.
[0440] The structure of the (meth)acrylate compound used in the Example is shown below.
[0441]
[0442]
[0443] MA-1 was synthesized by the synthesis method described in the patent document (WO2011-084546).
[0444] MA-2 was synthesized by the synthesis method described in the patent document (Japanese Patent Laid-Open No. 9-118717).
[0445] MA-3 was synthesized by the same synthesis method as MA-2.
[0446] MA-4 to MA-8 are novel compounds not disclosed in literature etc., and the synthesis method will be described in detail below.
[0447] MA-9 was synthesized by the synthesis method described in the patent document (Japanese Patent Laid-Open No. 2006-308878).
[0448] The products described in the following synthesis examples 1 to 5 were obtained by 1 H-NMR analysis and identification (analysis conditions are as follows).
[044...
Synthetic example 1MA-4
[0452]
[0453]
[0454]
[0455]In tetrahydrofuran (393.5g), put ethyl 4-bromobenzoate (78.7g, 344mmol), diethylamine (125.8g), 5-hexyn-1-ol (43.8g) and copper iodide (2.6g ), after forming a nitrogen atmosphere, bis(triphenylphosphine)palladium dichloride (4.8 g) was added, and the mixture was reacted at 60° C. for 7 hours. After the reaction was completed, 3.9 g of activated carbon (brand: JapanEnviroChemicals, Limited, specially made Bailu dry product) was added, stirred at room temperature for 1 hour, and then the activated carbon was removed by filtration. Next, tetrahydrofuran was removed by concentration under reduced pressure, diluted with ethyl acetate, and washed three times with pure water. Add 3.9 g of activated carbon (brand: Japan EnviroChemicals, Limited), a special dried egret product, to the resulting organic phase, stir at room temperature for 1 hour, filter, and concentrate under reduced pressure to obtain 103 g of MA-4A (crude yield: 122 %, traits:...
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