Nanometer anti-corrosion thermal insulation coating
A kind of thermal insulation coating, nano technology, applied in anti-corrosion coatings, fire-retardant coatings, coatings and other directions, to improve the bonding force, improve thermal insulation performance, and shield thermal energy.
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Embodiment 1
[0026] The preparation method of modified nano titanium nitride comprises the following steps:
[0027] Dissolve sodium lauryl sulfate in hot water at 70°C for stirring and dispersing, then add nano-titanium nitride for stirring and dispersing, ultrasonically treat for 1.5 hours, and then filter and dry to obtain modified nano-titanium nitride. The mass ratio of sodium lauryl sulfate to nano-titanium nitride is 7:1.
[0028] The effect of modification is measured by sedimentation experiment. Weigh 1-1.5g of the above-mentioned modified nano-titanium nitride sample and place it in a graduated cylinder with a ground mouth. First add a small amount of xylene to fully wet the nano-titanium nitride-graphene oxide. Finally, add xylene until 20mL is fully vibrated evenly, let it stand for different times under room temperature, record the mass of the sediment, and convert it into a sedimentation index; the sedimentation index=(mass of the sedimented part of the sample / total sample ma...
Embodiment 2
[0035] The preparation method of modified nano titanium nitride comprises the following steps:
[0036] Dissolve sodium lauryl sulfate in hot water at 80°C for stirring and dispersing, then add nano-titanium nitride for stirring and dispersing, ultrasonically treat for 0.5h, and then filter and dry to obtain modified nano-titanium nitride. The mass ratio of sodium lauryl sulfate to nano-titanium nitride is 5:1.
[0037] It can be seen from the test that the unmodified nano-titanium nitride-graphene oxide will completely settle down in xylene for about 3-5 hours, while the modified nano-titanium nitride will only settle in 1.2-1.8 hours after 24 hours in xylene. % precipitation, only about 2.6-3.2% precipitation after 48h. Therefore, the modified nano-titanium nitride has better dispersion performance and better modification effect.
[0038] The preparation method of modified silicone resin comprises the following steps:
[0039] 1) Calculated in parts by weight, weigh 50 pa...
Embodiment 3
[0043] A nano anti-corrosion thermal insulation coating, calculated in parts by weight, comprises the following components:
[0044] 50 parts of acrylic resins, 24 parts of modified silicone resins of Example 1, 9 parts of modified nano-titanium nitrides of Example 1, 7 parts of bentonite, 12 parts of nano ceramic hollow particles, 13 parts of graphite powder, alcohol ester twelve parts 4 parts, 0.3 parts of sodium oleate, 0.9 parts of pigment, 0.3 parts of emulsified methyl silicone oil and 25 parts of water.
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