Preparation method of fireproof material
A refractory material and refractory technology, applied in the field of refractory materials, can solve problems such as reducing the service life of refractory materials, increasing the damage rate of refractory products, and affecting thermal shock resistance, so as to improve thermal shock resistance, small reburning line changes, Effect of low thermal expansion coefficient
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Embodiment 1
[0024] A method for preparing a refractory material, comprising the following preparation steps:
[0025] a. Mix the carbonaceous material, refractory base material and alumina into a ball mill tank for 3 hours, then add an organic solvent, and stir evenly to obtain a slurry;
[0026] b. Mix partly stabilized zirconia, zirconium carbide particles, acrylic amine, methylenebisacrylamide and ammonium persulfate, introduce it into a high mixer, stir at a speed of 3000r / min for 10-15min, and then use ultrasonic oscillation for 20min , after uniform dispersion, material 1 was obtained;
[0027] c. Add catalyst and binder to material 1, stir and dissolve at 60°C for 10 minutes, then introduce the slurry, heat and stir at 90°C for 20 minutes to obtain a green body;
[0028] d. Put the green body in a constant temperature drying oven at 70°C, dry it for 20 minutes, crush it to pass through a 200-mesh sieve, perform secondary drying treatment, and then cool it and press it to form a fi...
Embodiment 2
[0037] A method for preparing a refractory material, comprising the following preparation steps:
[0038] a. Mix the carbonaceous material, refractory base material and alumina into a ball mill tank for 3 hours, then add an organic solvent, and stir evenly to obtain a slurry;
[0039] b. Mix partly stabilized zirconia, zirconium carbide particles, acrylic amine, methylenebisacrylamide and ammonium persulfate, introduce into a high-mixer, stir at a speed of 2000r / min for 10min, and then use ultrasonic oscillation for 20min to disperse After uniformity, material 1 is obtained;
[0040] c. Add catalyst and binder to material 1, stir and dissolve at 60°C for 5 minutes, then introduce the slurry, heat and stir at 80°C for 20 minutes to obtain a green body;
[0041] d. Put the green body in a constant temperature drying oven at 60°C, dry it for 15 minutes, crush it to pass through a 200-mesh sieve, perform secondary drying treatment, and then cool it and press it to form a finished...
Embodiment 3
[0050]A method for preparing a refractory material, comprising the following preparation steps:
[0051] a. Mix the carbonaceous material, refractory base material and alumina into a ball mill tank for 5 hours, then add an organic solvent, and stir evenly to obtain a slurry;
[0052] b. Mix partly stabilized zirconia, zirconium carbide particles, acrylic amine, methylene bisacrylamide and ammonium persulfate, introduce into a high-mixer, stir at a speed of 3000r / min for 15min, and then use ultrasonic oscillation for 25min to disperse After uniformity, material 1 is obtained;
[0053] c. Add catalyst and binder to material 1, stir and dissolve at 80°C for 10 minutes, then introduce the slurry, heat and stir at 90°C for 25 minutes to obtain a green body;
[0054] d. Put the green body in a constant temperature drying oven at 70°C, dry it for 20 minutes, crush it to pass through a 300-mesh sieve, perform secondary drying treatment, and then cool it and press it to form a finishe...
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