Preparation method of high-temperature-resistant easily-stripped printing water-emulsion type resin
An easy-to-peel, water-emulsion-type technology, used in coatings, paper coatings, textiles and papermaking, etc., can solve the problems of poor film-forming properties, unenvironmental protection, and poor high temperature resistance, so as to improve heat resistance and overcome heat resistance. The effect of poor performance and good transparency
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[0026] It should be noted that the structures, proportions, sizes, etc. shown in the drawings attached to this specification are only used to match the content disclosed in the specification, for those who are familiar with this technology to understand and read, and are not used to limit the implementation of the present invention Any modification of the structure, change of the proportional relationship or adjustment of the size shall still fall within the scope of the technical content disclosed in the present invention without affecting the effect and purpose of the present invention. In the range.
[0027] At the same time, terms such as "upper", "lower", "left", "right", "middle" and "one" quoted in this specification are only for the convenience of description and are not used to limit this specification. The practicable scope of the invention and the change or adjustment of its relative relationship shall also be regarded as the practicable scope of the present inventi...
Embodiment 1
[0029] The invention discloses a preparation method of high-temperature-resistant and easy-peeling printing water-emulsion resin, which comprises the following steps:
[0030] Step 1) configuring an aqueous emulsion of a nonionic emulsifier and an anionic emulsifier;
[0031] Step 2) Adding a low-temperature initiator to the aqueous emulsion in step 1) under stirring conditions and feeding nitrogen gas, and adding the monomer with a high glass transition temperature to the aqueous emulsion at a uniform speed and slowly within 4h to 7h;
[0032] Step 3) preparing high glass transition temperature resin seed emulsion;
[0033] Step 4) Use a pump to pump the medium-high glass transition temperature resin seed emulsion in step 3) into the pre-emulsified nano-oxide dispersion, and react to obtain a high-temperature resistant and easy-to-peel printing water-emulsion resin.
Embodiment 2
[0035] The invention discloses a preparation method of high-temperature-resistant and easy-peeling printing water-emulsion resin, which comprises the following steps:
[0036] Step 1) configuring an aqueous emulsion of a nonionic emulsifier and an anionic emulsifier;
[0037] Step 2) Adding a low-temperature initiator to the aqueous emulsion in step 1) under stirring conditions and feeding nitrogen gas, and adding the monomer with a high glass transition temperature to the aqueous emulsion at a uniform speed and slowly within 4h to 7h;
[0038] Step 3) preparing high glass transition temperature resin seed emulsion;
[0039] Step 4) Use a pump to pump the medium-high glass transition temperature resin seed emulsion in step 3) into the pre-emulsified nano-oxide dispersion, and react to obtain a high-temperature resistant and easy-to-peel printing water-emulsion resin.
[0040] Preferably, a method for preparing a high-temperature-resistant and easy-to-peel printing water-emuls...
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