Self circulation array pipe reaction device with efficient mixer and reaction method using same

Abstract

The invention relates to a self circulation array pipe reaction device with an efficient mixer and a reaction method using the same. The material mixing problem is solved through the arrangement of anefficient mixer and a circulation pump. The heat transfer problem and the reaction flux problem can be effectively solved in time through installing an array pipe reactor and controlling the circulation quantity. The reaction device provided by the invention has the advantages that the heat transfer effect is good; the material mixing is uniform; the continuous and automatic reaction can be realized. The reaction method using the reaction device provided by the invention has the advantages that the operation is simple; the reaction efficiency is high; the heat transfer effect is good; side reactions are few; the reaction flux is great.

Description

technical field [0001] The invention relates to the field of reactors, in particular to a self-circulating tubular reaction device with a high-efficiency mixer and a reaction method using the same. Background technique [0002] Gas-liquid, liquid-liquid and liquid-solid phase reactions are often encountered in chemical synthesis production, so reaction devices are required. The most widely used type of reaction equipment is the tank reactor. [0003] Tank reactors (reactors) are used to carry out many different reaction processes, but the reactors have the following disadvantages: limited volume, suitable for batch reactions, and often require a combination of multiple tanks; the larger the diameter of the reactor, the more materials in the tank are stirred and mixed Inhomogeneous, poor mixing effect; in different stages of the reaction, the energy generated is different, which is not conducive to operation control; the larger the reactor, the smaller the specific surface ar...

AI Technical Summary

Problems solved by technology

[0003] Tank reactors (reactors) are used to carry out many different reaction processes, but the reactors have the following disadvantages: limited volume, suitable for batch reactions, and often require a combination of multiple tanks; the larger the diameter of the reactor, the more materials in the tank are stirred and mixed Inhomogeneous, poor mixing effect; in different stages of the reaction, the energy generated is different, which is not conducive to operation control; the larger the reactor, the smaller the specific surface area, low heat transfer efficiency, difficult temperature control, especially rapid reaction and severe heat release, etc. The reaction can easily cause safety problems because the heat cannot be removed in time; the material is in the kettle for a long time, which is prone to side reactions; the stirring power system needs maintenance and is difficult to replace

[0004] Microchannel reactors can solve the problem of heat removal in terms of heat transfer. The heat transfer efficiency is 5-100 times that of tank reactors. However, it has problems such as high processing precision, high cost, small flux, and limited applicable reaction types. Cannot be widely promoted

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