Inorganic non-linear optical crystal sodium iodobismuthate, and preparation and application thereof
An inorganic and crystal technology, applied in the field of inorganic crystal optical materials, can solve the problems of difficult to withstand high-intensity laser irradiation, low laser damage threshold, harsh synthesis conditions, etc., and achieve stable air, mild experimental conditions, and high raw material utilization. Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0026] 2mmol NaIO 4 , 2mmol NaCl, 0.5mmol Bi 2 o 3 and 3 mmol H 5 IO 6 Add it into a hydrothermal reaction kettle with a volume of 23mL, and then add 3mL of distilled water to make the final concentration of NaCl 0.6mol / L; seal the hydrothermal reaction kettle and put it in a muffle furnace, heat it to 230°C for 3 hours, and react at a constant temperature for 4 Then cool down to room temperature at a cooling rate of 8°C / h; after the reaction, the product is suction filtered and the solid is washed with deionized water and ethanol successively, and dried to obtain the inorganic crystal compound NaBi(IO 3 ) 4 .
Embodiment 2
[0028] 2mmol NaIO 4 , 2mmol NaCl, 0.1mmol Bi 2 o 3 and 2 mmol H 5 IO 6 Add it into a hydrothermal reaction kettle with a volume of 23mL, and then add 3mL of distilled water to make the final concentration of NaCl 0.6mol / L; seal the hydrothermal reaction kettle and put it in a muffle furnace, heat it to 250°C for 3 hours, and react at a constant temperature for 2 Then cool down to room temperature at a cooling rate of 8° C. / h; after the reaction, the product is suction filtered and washed with deionized water and ethanol successively to obtain a solid, and dried to obtain the inorganic crystal compound NaBi(IO 3 ) 4 .
Embodiment 3
[0030] 2mmol NaIO 4 , 2mmol NaCl, 0.2mmol (BiO) 2 CO 3 and 3 mmol HIO 3 Add it into a hydrothermal reaction kettle with a volume of 23mL, and then add 2mL of distilled water to make the final concentration of NaCl 1mol / L; seal the hydrothermal reaction kettle and put it in a muffle furnace, heat it to 210°C for 3 hours, and react at a constant temperature for 4 days Then cool down to room temperature at a cooling rate of 1° C. / h; after the reaction is over, the product is suction-filtered and washed with deionized water and ethanol successively to obtain a solid, and dried to obtain the inorganic crystal compound NaBi(IO 3 ) 4 .
[0031]The frequency doubling performance and phase matching test of the inorganic crystal compound prepared in the present invention are obtained by the Kurtz powder frequency doubling test method. The specific operation steps are as follows: the obtained inorganic crystal compound is firstly ground and sieved into powders of different particle ...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com