Graphene-modified polyethylene terephthalate resin
A technology of polyethylene terephthalate and ethylene terephthalate, which is applied in the field of reinforced polymer materials and graphene-modified polyethylene terephthalate resin, can solve the problem of heavy metal back cover, It is free from the problems of fashion and thinness, and the mobile phone feels cumbersome to hold, and achieves the effect of firm combination, good glossy texture and good combination effect.
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Embodiment 1
[0040] A graphene-modified polyethylene terephthalate resin, containing 5wt% graphene in the polyethylene terephthalate resin.
Embodiment 2
[0042] A graphene-modified polyethylene terephthalate resin, containing 2wt% graphene in the polyethylene terephthalate resin. The preparation method is as follows:
[0043] (1) Dissolve graphene in ethanol, and stir for 20 minutes at a speed above 3000r / min, so that the material liquid is evenly dispersed.
[0044] (2) Then add polyethylene terephthalate masterbatch granules to the feed liquid, continue to stir for 5 minutes, transfer to a drum dryer, and drum dry.
[0045] (3) The dried material is heated and melted under nitrogen protection, and finally cooled to obtain a graphene-modified polyethylene terephthalate resin.
Embodiment 3
[0047] A graphene-modified polyethylene terephthalate resin, containing 3wt% modified graphene in the polyethylene terephthalate resin. The modified graphene is modified by using humic acid, and the modification process is as follows: take humic acid, add 3 times the weight of 20v% ethanol solution, stir for 10 minutes, filter and retain the filter residue; add 10 times the weight of the second Diethanol solution, add graphene (4 times weight with respect to humic acid), 3000r / min stirs 15min, obtains humic acid composite graphene feed liquid.
[0048] The process of preparing graphene-modified polyethylene terephthalate is as follows:
[0049]Add polyethylene terephthalate masterbatch granule to above-mentioned humic acid composite graphene feed liquid, continue to stir 5min, transfer in the tumble drier, tumble dry. The dried material is heated and melted under the protection of nitrogen, and finally cooled to obtain a graphene-modified polyethylene terephthalate resin.
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