Process for directly preparing oxygen-free copper from waste red impure copper
A technology of oxygen-free copper and red miscellaneous copper, which is applied in the technical field of directly preparing oxygen-free copper from waste red miscellaneous copper, can solve the problem that oxygen-free copper products cannot be produced, and cannot be used to draw small copper wires or fine copper wires. , micro-wire copper products, etc.
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Embodiment 1
[0027] Use a tilting furnace to smelt waste red copper with a copper content of 96%wt, and use oxy-fuel combustion and natural gas reduction. At the end of the reduction, a rare earth refining agent is used to remove impurities, deoxidize, and purify the copper liquid. The oxygen content of the copper liquid after reduction The copper content is 300ppm, and the copper content is 99.93%; the temperature of the copper liquid is maintained at 1150°C, and the rare earth refining agent is La-Ce series, in which the content of lanthanum (La) is 35% and that of cerium (Ce) is 65%. Then put the molten copper into a closed static furnace that relies on electric heating and heat preservation. The refining furnace and the static furnace are connected by a sealed launder, and the straight line distance of the connection is 1200mm. The graphite material in the sealed launder is used to contact the copper liquid; There is an oval charcoal filter bag at the end (at the exit of the furnace) to...
Embodiment 2
[0029] Use a fixed reverberatory furnace to smelt waste red copper with a copper content of 96.6%wt, and use oxy-fuel combustion and natural gas reduction. At the end of the reduction, a rare earth refining agent is used to remove impurities, deoxidize, and purify the copper liquid. The copper liquid after reduction The oxygen content is 280ppm, the copper content is 99.96%; the temperature of the copper liquid is maintained at 1160°C, and the rare earth refining agent is La-Ce series, in which the content of lanthanum (La) is 35% and that of cerium (Ce) is 65%. Then put the molten copper into a closed static furnace that relies on electric heating and heat preservation. The refining furnace and the static furnace are connected by a sealed launder, and the straight-line distance of the connection is 1150mm. The graphite material in the sealed launder is used to contact the copper liquid; the sealed launder There is an oval charcoal filter bag at the end (at the exit of the furn...
Embodiment 3
[0031] Use NGL furnace to smelt waste red copper with a copper content of 96.5%wt, and use oxy-fuel combustion and natural gas reduction. At the end of the reduction, rare earth refining agents are used to remove impurities, deoxidize, and purify the copper liquid. The oxygen content of the copper liquid after reduction The copper content is 250ppm, and the copper content is 99.95%; the temperature of the copper liquid is kept at 1170°C, and the rare earth refining agent is La-Ce series, in which the content of lanthanum (La) is 35% and that of cerium (Ce) is 65%. Then put the molten copper into a closed static furnace that relies on electric heating and heat preservation. The refining furnace and the static furnace are connected by a sealed launder, and the straight-line distance of the connection is 1135mm. There is an oval charcoal filter bag at the end (at the exit of the furnace) to further deoxidize the copper liquid during filtration. The copper liquid in the electric h...
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